Journal Published Online: 01 April 1986
Volume 31, Issue 2

Spectral Differentiation and Gas Chromatographic/Mass Spectrometric Analysis of the Lacrimators 2-Chloroacetophenone and -Chlorobenzylidene Malononitrile

CODEN: JFSCAS

Abstract

2-Chloroacetophenone (CN) and o-chlorobenzylidene malononitrile (CS) are the most common chemical agents used as lacrimators in the United States. There is a lack of complete spectral data on these compounds in the literature. Spectral data (ultraviolet, fluorescence, proton nuclear magnetic resonance, and infrared) and a gas-liquid chromatographic/mass spectrometric method are presented that differentiate and identify CN and CS. These methods and data were used to identify a forensic science specimen from an accidental intoxication.

Author Information

Ferslew, KE
Quillen-Dishner College of Medicine, East Tennessee State University, Johnson City, TN
Orcutt, RH
East Tennessee State University, Johnson City, TN
Hagardorn, AN
Quillen-Dishner College of Medicine, East Tennessee State University, Johnson City, TN
Pages: 8
Price: $25.00
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Stock #: JFS12298J
ISSN: 0022-1198
DOI: 10.1520/JFS12298J