ASTM G67 - 18

    Standard Test Method for Determining the Susceptibility to Intergranular Corrosion of 5XXX Series Aluminum Alloys by Mass Loss After Exposure to Nitric Acid (NAMLT Test)

    Active Standard ASTM G67 | Developed by Subcommittee: G01.05

    Book of Standards Volume: 03.02


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    Significance and Use

    4.1 This test method provides a quantitative measure of the susceptibility to intergranular corrosion of Al-Mg and Al-Mg-Mn alloys. The nitric acid dissolves a second phase, an aluminum-magnesium intermetallic compound (βAl-Mg), in preference to the solid solution of magnesium in the aluminum matrix. When this compound is precipitated in a relatively continuous network along grain boundaries, the effect of the preferential attack is to corrode around the grains, causing them to fall away from the specimens. Such dropping out of the grains causes relatively large mass losses of the order of 25 to 75 mg/cm2 (160 to 480 mg/in.2), whereas, samples of intergranular-resistant materials lose only about 1 to 15 mg/cm2 (10 to 100 mg/in.2). When the βAl-Mg compound is randomly distributed, the preferential attack can result in intermediate mass losses. Metallographic examination is required in such cases to establish whether or not the loss in mass is the result of intergranular attack.

    4.2 The precipitation of the second phase in the grain boundaries also gives rise to intergranular corrosion when the material is exposed to chloride-containing natural environments, such as seacoast atmospheres or sea water. The extent to which the alloy will be susceptible to intergranular corrosion depends upon the degree of precipitate continuity in the grain boundaries. Visible manifestations of the attack may be in various forms such as pitting, exfoliation, or stress-corrosion cracking, depending upon the morphology of the grain structure and the presence of sustained tensile stress.3

    1. Scope

    1.1 This test method, also known as the Nitric Acid Mass Loss Test (NAMLT) describes a procedure for constant immersion intergranular corrosion testing of 5XXX series aluminum alloys.

    1.2 This test method is applicable only to wrought products.

    1.3 This test method covers type of specimen, specimen preparation, test environment, and method of exposure.

    1.4 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.

    1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.

    1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.


    2. Referenced Documents (purchase separately) The documents listed below are referenced within the subject standard but are not provided as part of the standard.

    ASTM Standards

    D1193 Specification for Reagent Water

    E29 Practice for Using Significant Digits in Test Data to Determine Conformance with Specifications

    E691 Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method

    G1 Practice for Preparing, Cleaning, and Evaluating Corrosion Test Specimens

    G16 Guide for Applying Statistics to Analysis of Corrosion Data


    ICS Code

    ICS Number Code 77.120.10 (Aluminium and aluminium alloys)

    UNSPSC Code

    UNSPSC Code 11172000(Aluminum based alloys)


    Referencing This Standard
    Link Here
    Link to Active (This link will always route to the current Active version of the standard.)

    DOI: 10.1520/G0067-18

    Citation Format

    ASTM G67-18, Standard Test Method for Determining the Susceptibility to Intergranular Corrosion of 5XXX Series Aluminum Alloys by Mass Loss After Exposure to Nitric Acid (NAMLT Test), ASTM International, West Conshohocken, PA, 2018, www.astm.org

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