ASTM D7279 - 18
Standard Test Method for Kinematic Viscosity of Transparent and Opaque Liquids by Automated Houillon Viscometer
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Significance and Use
4.1 Many petroleum products and some non-petroleum products are used as lubricants in the equipment, and the correct operation of the equipment depends upon the appropriate viscosity of the lubricant being used. Additionally, the viscosity of many petroleum fuels is important for the estimation of optimum storage, handling, and operational conditions. Thus, the accurate determination of viscosity is essential to many product specifications.
4.2 The viscosity of used oils is a commonly determined parameter in the oil industry to assess the effect of engine wear on the lube oils used, as well as the degradation of the engine parts during operation.
4.3 The Houillon viscometer tube method offers automated determination of kinematic viscosity. Typically a sample volume of less than 1 mL is required for the analysis.
1. Scope
1.1 This test method covers the measurement of the kinematic viscosity of transparent and opaque liquids; such as base oils, formulated oils, diesel oil, biodiesel, biodiesel blends, residual fuel oils, marine fuels, and used lubricating oils using a Houillon viscometer in automated mode.
1.2 The range of kinematic viscosity capable of being measured by this test method is from 2 mm2/s to 2500 mm2/s (see Fig. 1). The range is dependent on the tube constant utilized. The temperature range that the apparatus is capable of achieving is between 20 °C and 150 °C, inclusive. However, the precision has only been determined for the viscosity range; 2 mm2/s to 478 mm2/s at 40 °C for base oils, formulated oils, diesel oil, biodiesel, and biodiesel blends; 3 mm2/s to 106 mm2/s at 100 °C for base oils and formulated oils; 25 mm2/s to 150 mm2/s at 40 °C and 5 mm2/s to 16 mm2/s at 100 °C for used lubricating oils; 25 mm2/s to 2500 mm2/s at 50 °C and 6 mm2/s to 110 mm2/s at 100 °C for residual fuels. As indicated for the materials listed in the precision section.
FIG. 1 Houillon Viscometer Typical Viscosity Range of Tube Constants
Note 1: Viscosity range of a Houillon tube is based on most practical flow time of 30 s to 200 s.
1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For specific warning statements, see Section 6.
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
2. Referenced Documents (purchase separately) The documents listed below are referenced within the subject standard but are not provided as part of the standard.
ASTM Standards
D445 Test Method for Kinematic Viscosity of Transparent and Opaque Liquids (and Calculation of Dynamic Viscosity)
D2162 Practice for Basic Calibration of Master Viscometers and Viscosity Oil Standards
D4057 Practice for Manual Sampling of Petroleum and Petroleum Products
D4177 Practice for Automatic Sampling of Petroleum and Petroleum Products
D6299 Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
D6300 Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants
D6708 Practice for Statistical Assessment and Improvement of Expected Agreement Between Two Test Methods that Purport to Measure the Same Property of a Material
D6792 Practice for Quality Management Systems in Petroleum Products, Liquid Fuels, and Lubricants Testing Laboratories
D7962 Practice for Determination of Minimum Immersion Depth and Assessment of Temperature Sensor Measurement Drift
E563 Practice for Preparation and Use of an Ice-Point Bath as a Reference Temperature
E644 Test Methods for Testing Industrial Resistance Thermometers
E1750 Guide for Use of Water Triple Point Cells
E2877 Guide for Digital Contact Thermometers
NIST Standard
NIST Technical Note 1297 Guideline for Evaluating and Expressing the Uncertainty of NIST Measurement Results Available from National Institute of Standards and Technology (NIST), 100 Bureau Dr., Stop 1070, Gaithersburg, MD 20899-1070, http://www.nist.gov.ISO Standards
ISO 5725 Accuracy (Trueness and Precision) of Measurement Methods and Results Available from American National Standards Institute (ANSI), 25 W. 43rd St., 4th Floor, New York, NY 10036, http://www.ansi.org.ICS Code
ICS Number Code 17.060 (Measurement of volume, mass, density, viscosity); 75.100 (Lubricants, industrial oils and related products)
Referencing This Standard
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DOI: 10.1520/D7279-18
Citation Format
ASTM D7279-18, Standard Test Method for Kinematic Viscosity of Transparent and Opaque Liquids by Automated Houillon Viscometer, ASTM International, West Conshohocken, PA, 2018, www.astm.org
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