ASTM D6751 - 15ce1
Standard Specification for Biodiesel Fuel Blend Stock (B100) for Middle Distillate Fuels
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Abstract
This specification covers biodiesel fuel blend stock, B100, in Grades S15 and S500 for use as a blend component with middle distillate fuels. This specification prescribes the required properties of diesel fuels at the time and place of delivery. The requirements stated here may be applied at other points in the production and distribution system when provided by agreement between the purchaser and the supplier. The biodiesel specified shall be mono-alkyl esters of long chain fatty acids derived from vegetable oils and animal fats. The product shall undergo chemical analysis for flash point, methanol, water and sediment, kinematic viscosity, sulfated ash, oxidation stability, sulfur, copper strip corrosion, cetane number, cloud point, acid number, carbon residue, total and free glycerin, phosphorus, reduce pressure distillation temperature, atmospheric equivalent temperature, combined calcium and magnesium, and combined sodium and magnesium.
This abstract is a brief summary of the referenced standard. It is informational only and not an official part of the standard; the full text of the standard itself must be referred to for its use and application. ASTM does not give any warranty express or implied or make any representation that the contents of this abstract are accurate, complete or up to date.
1. Scope
1.1 This specification covers four grades of biodiesel (B100) for use as a blend component with middle distillate fuels. These grades are described as follows:
1.1.1 Grade No. 1-B S15—A special purpose biodiesel blendstock intended for use in middle distillate fuel applications which can be sensitive to the presence of partially reacted glycerides, including those applications requiring good low temperature operability, and also requiring a fuel blend component with 15 ppm sulfur (maximum).
1.1.2 Grade No. 1-B S500—A special purpose biodiesel blendstock intended for use in middle distillate fuel applications which can be sensitive to the presence of partially reacted glycerides, including those applications requiring good low temperature operability, and also requiring a fuel blend component with 500 ppm sulfur (maximum).
1.1.3 Grade No. 2-B S15—A general purpose biodiesel blendstock intended for use in middle distillate fuel applications that require a fuel blend component with 15 ppm sulfur (maximum).
1.1.4 Grade No. 2-B S500—A general purpose biodiesel blendstock intended for use in middle distillate fuel applications that require a fuel blend component with 500 ppm sulfur (maximum).
1.2 This specification prescribes the required properties of diesel fuels at the time and place of delivery. The specification requirements may be applied at other points in the production and distribution system when provided by agreement between the purchaser and the supplier.
1.3 Nothing in this specification shall preclude observance of federal, state, or local regulations which may be more restrictive.
Note 1: The generation and dissipation of static electricity can create problems in the handling of distillate fuel oils with which biodiesel may be blended. For more information on the subject, see Guide D4865.
1.4 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
2. Referenced Documents (purchase separately) The documents listed below are referenced within the subject standard but are not provided as part of the standard.
ASTM Standards
D93 Test Methods for Flash Point by Pensky-Martens Closed Cup Tester
D130 Test Method for Corrosiveness to Copper from Petroleum Products by Copper Strip Test
D189 Test Method for Conradson Carbon Residue of Petroleum Products
D445 Test Method for Kinematic Viscosity of Transparent and Opaque Liquids (and Calculation of Dynamic Viscosity)
D524 Test Method for Ramsbottom Carbon Residue of Petroleum Products
D613 Test Method for Cetane Number of Diesel Fuel Oil
D664 Test Method for Acid Number of Petroleum Products by Potentiometric Titration
D874 Test Method for Sulfated Ash from Lubricating Oils and Additives
D974 Test Method for Acid and Base Number by Color-Indicator Titration
D975 Specification for Diesel Fuel Oils
D976 Test Method for Calculated Cetane Index of Distillate Fuels
D1160 Test Method for Distillation of Petroleum Products at Reduced Pressure
D1266 Test Method for Sulfur in Petroleum Products (Lamp Method)
D1796 Test Method for Water and Sediment in Fuel Oils by the Centrifuge Method (Laboratory Procedure)
D2274 Test Method for Oxidation Stability of Distillate Fuel Oil (Accelerated Method)
D2500 Test Method for Cloud Point of Petroleum Products
D2622 Test Method for Sulfur in Petroleum Products by Wavelength Dispersive X-ray Fluorescence Spectrometry
D2709 Test Method for Water and Sediment in Middle Distillate Fuels by Centrifuge
D2880 Specification for Gas Turbine Fuel Oils
D3117 Test Method for Wax Appearance Point of Distillate Fuels
D3120 Test Method for Trace Quantities of Sulfur in Light Liquid Petroleum Hydrocarbons by Oxidative Microcoulometry
D3242 Test Method for Acidity in Aviation Turbine Fuel
D3828 Test Methods for Flash Point by Small Scale Closed Cup Tester
D4057 Practice for Manual Sampling of Petroleum and Petroleum Products
D4177 Practice for Automatic Sampling of Petroleum and Petroleum Products
D4294 Test Method for Sulfur in Petroleum and Petroleum Products by Energy Dispersive X-ray Fluorescence Spectrometry
D4530 Test Method for Determination of Carbon Residue (Micro Method)
D4737 Test Method for Calculated Cetane Index by Four Variable Equation
D4865 Guide for Generation and Dissipation of Static Electricity in Petroleum Fuel Systems
D4951 Test Method for Determination of Additive Elements in Lubricating Oils by Inductively Coupled Plasma Atomic Emission Spectrometry
D5453 Test Method for Determination of Total Sulfur in Light Hydrocarbons, Spark Ignition Engine Fuel, Diesel Engine Fuel, and Engine Oil by Ultraviolet Fluorescence
D5771 Test Method for Cloud Point of Petroleum Products (Optical Detection Stepped Cooling Method)
D5772 Test Method for Cloud Point of Petroleum Products (Linear Cooling Rate Method)
D5773 Test Method for Cloud Point of Petroleum Products (Constant Cooling Rate Method)
D6217 Test Method for Particulate Contamination in Middle Distillate Fuels by Laboratory Filtration
D6450 Test Method for Flash Point by Continuously Closed Cup (CCCFP) Tester
D6469 Guide for Microbial Contamination in Fuels and Fuel Systems
D6584 Test Method for Determination of Total Monoglycerides, Total Diglycerides, Total Triglycerides, and Free and Total Glycerin in B-100 Biodiesel Methyl Esters by Gas Chromatography
D6890 Test Method for Determination of Ignition Delay and Derived Cetane Number (DCN) of Diesel Fuel Oils by Combustion in a Constant Volume Chamber
D7039 Test Method for Sulfur in Gasoline, Diesel Fuel, Jet Fuel, Kerosine, Biodiesel, Biodiesel Blends, and Gasoline-Ethanol Blends by Monochromatic Wavelength Dispersive X-ray Fluorescence Spectrometry
D7344 Test Method for Distillation of Petroleum Products and Liquid Fuels at Atmospheric Pressure (Mini Method)
D7345 Test Method for Distillation of Petroleum Products and Liquid Fuels at Atmospheric Pressure (Micro Distillation Method)
D7397 Test Method for Cloud Point of Petroleum Products (Miniaturized Optical Method)
D7501 Test Method for Determination of Fuel Filter Blocking Potential of Biodiesel (B100) Blend Stock by Cold Soak Filtration Test (CSFT)
D7668 Test Method for Determination of Derived Cetane Number (DCN) of Diesel Fuel OilsIgnition Delay and Combustion Delay Using a Constant Volume Combustion Chamber Method
D7689 Test Method for Cloud Point of Petroleum Products (Mini Method)
Government Standard
40 CFR Part 79 Registration of Fuels and Fuel Additives Section 211(b) Clean Air Act Available from U.S. Government Printing Office Superintendent of Documents, 732 N. Capitol St., NW, Mail Stop: SDE, Washington, DC 20401.Other Documents
AOCS Standard Procedure Ck 2-09 Available from AO EN 14105 Fat and Oil DerivativesFatty Acid Methyl Esters (FAME)Determination of Free and Total Glycerol and Mono-, Di-, Triglyceride Contents (Reference Method) Available from the National CEN Members listed on the CEN website (www.cenorm.be) or from the CEN/TC19 secretariat (astm@nen.nl). EN 14538 Fat and Oil DerivativesFatty Acid Methyl Esters (FAME)Determination of Ca, K, Mg and Na Content by Optical Emission Spectral Analysis with Inductively Coupled Plasma (ICP OES) EN 15751 Automotive FuelsFatty Acid Methyl Ester (FAME) Fuel and Blends with Diesel FuelDetermination of Oxidation Stability by Accelerated Oxidation Method UOP 389 Trace Metals in Oils by Wet Ashing and ICP-OES Available from ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA. Visit the ASTM website, www.astm.org, or contact ASTM Customer Service at service@astm.org.ICS Code
ICS Number Code 75.160.20 (Liquid fuels)
Referencing This Standard
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DOI: 10.1520/D6751-15CE01
Citation Format
ASTM D6751-15ce1, Standard Specification for Biodiesel Fuel Blend Stock (B100) for Middle Distillate Fuels, ASTM International, West Conshohocken, PA, 2015, www.astm.org
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