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Significance and Use
5.1 Ash, as determined by this test method, is the residue remaining after burning the coal and coke. Ash obtained differs in composition from the inorganic constituents present in the original coal. Incineration causes an expulsion of all water, the loss of carbon dioxide from carbonates, the conversion of iron pyrites into ferric oxide, and other chemical reactions. Ash, as determined by this test method, will differ in amount from ash produced in furnace operations and other firing systems because incineration conditions influence the chemistry and amount of the ash. References for correcting ash results determined by this test method to a mineral-matter-free basis are listed in Classification , Section 9.
1.1 This test method covers the determination of the inorganic residue as ash in the analysis sample of coal or coke as prepared in accordance with Practice or Practice . The results obtained can be applied as the ash in the proximate analysis, Practice , and in the ultimate analysis, Practice . For the determination of the constituents in ash, reference is made to Test Methods , , and . Test Methods should be used to prepare ash to be used for trace element analysis. See Terminology for definition of ash.
1.2 The values stated in SI units are to be regarded as standard. The values given in parentheses after SI units are provided for information only and are not considered standard.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
2. Referenced Documents (purchase separately) The documents listed below are referenced within the subject standard but are not provided as part of the standard.
D121 Terminology of Coal and Coke
D346 Practice for Collection and Preparation of Coke Samples for Laboratory Analysis
D388 Classification of Coals by Rank
D1757 Test Method for Sulfate Sulfur in Ash from Coal and Coke
D2013 Practice for Preparing Coal Samples for Analysis
D2795 Test Methods for Analysis of Coal and Coke Ash
D3172 Practice for Proximate Analysis of Coal and Coke
D3173 Test Method for Moisture in the Analysis Sample of Coal and Coke
D3176 Practice for Ultimate Analysis of Coal and Coke
D3180 Practice for Calculating Coal and Coke Analyses from As-Determined to Different Bases
D3682 Test Method for Major and Minor Elements in Combustion Residues from Coal Utilization Processes
D4326 Test Method for Major and Minor Elements in Coal and Coke Ash By X-Ray Fluorescence
D5016 Test Method for Total Sulfur in Coal and Coke Combustion Residues Using a High-Temperature Tube Furnace Combustion Method with Infrared Absorption
D6349 Test Method for Determination of Major and Minor Elements in Coal, Coke, and Solid Residues from Combustion of Coal and Coke by Inductively Coupled Plasma--Atomic Emission Spectrometry
D6357 Test Methods for Determination of Trace Elements in Coal, Coke, and Combustion Residues from Coal Utilization Processes by Inductively Coupled Plasma Atomic Emission Spectrometry, Inductively Coupled Plasma Mass Spectrometry, and Graphite Furnace Atomic Absorption Spectro
E691 Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
ICS Number Code 75.160.10 (Solid fuels)
UNSPSC Code 15101601(Coal); 15101604(Coke)
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ASTM D3174-12(2018)e1, Standard Test Method for Ash in the Analysis Sample of Coal and Coke from Coal, ASTM International, West Conshohocken, PA, 2018, www.astm.orgBack to Top