ASTM E2554 - 13

    Standard Practice for Estimating and Monitoring the Uncertainty of Test Results of a Test Method Using Control Chart Techniques

    Active Standard ASTM E2554 | Developed by Subcommittee: E11.20

    Book of Standards Volume: 14.02


      Format Pages Price  
    PDF 7 $43.00   ADD TO CART
    Hardcopy (shipping and handling) 7 $43.00   ADD TO CART
    Standard + Redline PDF Bundle 14 $51.60   ADD TO CART


    Significance and Use

    4.1 This practice provides one way for a laboratory to develop data-based Type A estimates of uncertainty as referred to in Section A22 in Form and Style of ASTM Standards.

    4.2 Laboratories accredited under ISO/IEC 17025 are required to present uncertainty estimates for their test results. This practice provides procedures that use test results to develop uncertainty estimates for an individual laboratory.

    4.3 Generally, these test results will be from a single sample of stable and homogeneous material known as a control or check sample.

    4.4 The true value of the characteristic(s) of the control sample being measured will ordinarily be unknown. However, this methodology may also be used if the control sample is a reference material, in which case the test method bias may also be estimated and incorporated into the uncertainty estimate. Many test methods do not have true reference materials available to provide traceable chains of uncertainty estimation.

    4.5 This practice also allows for ongoing monitoring of the laboratory uncertainty. As estimates of the level of uncertainty change, possibly as contributions to uncertainty are identified and minimized, revision to the laboratory uncertainty will be possible.

    1. Scope

    1.1 This practice describes techniques for a laboratory to estimate the uncertainty of a test result using data from test results on a control sample. This standard provides one method for a laboratory to estimate Measurement Uncertainty in accordance with Section A22.3 in Form and Style of ASTM Standards.

    1.2 Uncertainty as defined by this practice applies to the capabilities of a single laboratory. Any estimate of uncertainty determined through the use of this practice applies only to the individual laboratory for which the data are presented.

    1.3 The laboratory uses a well defined and established test method in determining a series of test results. The uncertainty estimated using this practice only applies when the same test method is followed. The uncertainty only applies for the material types represented by the control samples, and multiple control samples may be needed, especially if the method has different precision for different sample types or response levels.

    1.4 The uncertainty estimate determined by this practice represents the intermediate precision of test results. This estimate seeks to quantify the total variation expected within a single laboratory using a single established test method while incorporating as many known sources of variation as possible.

    1.5 This practice does not establish error estimates (error budget) attributed to individual factors that could influence uncertainty.

    1.6 This practice describes the use of control charts to evaluate the data obtained and presents a special type of control chart to monitor the estimate of uncertainty.

    1.7 The system of units for this standard is not specified. Dimensional quantities in the standard are presented only as illustrations of calculation methods. The examples are not binding on products or test methods treated.

    1.8 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.


    2. Referenced Documents (purchase separately) The documents listed below are referenced within the subject standard but are not provided as part of the standard.

    ASTM Standards

    D5184 Test Methods for Determination of Aluminum and Silicon in Fuel Oils by Ashing, Fusion, Inductively Coupled Plasma Atomic Emission Spectrometry, and Atomic Absorption Spectrometry

    E177 Practice for Use of the Terms Precision and Bias in ASTM Test Methods

    E456 Terminology Relating to Quality and Statistics

    E2282 Guide for Defining the Test Result of a Test Method

    E2587 Practice for Use of Control Charts in Statistical Process Control

    ISO/ASTM51707 Guide for Estimating Uncertainties in Dosimetry for Radiation Processing

    ASTM Publications

    FormandStyleforASTMS

    ManualonPresentation 7th Edition

    ISO Standard

    ISO/IEC17025 General Requirements for the Competence of Testing and Calibration Laboratories


    ICS Code

    ICS Number Code 03.120.10 (Quality management and quality assurance); 19.020 (Test conditions and procedures in general)

    UNSPSC Code

    UNSPSC Code


    Referencing This Standard

    DOI: 10.1520/E2554-13

    ASTM International is a member of CrossRef.

    Citation Format

    ASTM E2554-13, Standard Practice for Estimating and Monitoring the Uncertainty of Test Results of a Test Method Using Control Chart Techniques, ASTM International, West Conshohocken, PA, 2013, www.astm.org

    Back to Top