Active Standard ASTM D3174 | Developed by Subcommittee: D05.21
Book of Standards Volume: 05.06
Historical (view previous versions of standard)
Significance and Use
5.1 Ash, as determined by this test method, is the residue remaining after burning the coal and coke. Ash obtained differs in composition from the inorganic constituents present in the original coal. Incineration causes an expulsion of all water, the loss of carbon dioxide from carbonates, the conversion of iron pyrites into ferric oxide, and other chemical reactions. Ash, as determined by this test method, will differ in amount from ash produced in furnace operations and other firing systems because incineration conditions influence the chemistry and amount of the ash. References for correcting ash results determined by this test method to a mineral-matter-free basis are listed in Classification D388, Section 9.
1.1 This test method covers the determination of the inorganic residue as ash in the analysis sample of coal or coke as prepared in accordance with Practice D2013 or Practice D346. The results obtained can be applied as the ash in the proximate analysis, Practice D3172, and in the ultimate analysis, Practice D3176. For the determination of the constituents in ash, reference is made to Test Methods D3682, D4326 and D6349. Test Method D6357 should be used to prepare ash to be used for trace element analysis. See Terminology D121 for definition of ash.
2. Referenced Documents (purchase separately) The documents listed below are referenced within the subject standard but are not provided as part of the standard.
D121 Terminology of Coal and Coke
D346 Practice for Collection and Preparation of Coke Samples for Laboratory Analysis
D388 Classification of Coals by Rank
D1757 Test Method for Sulfate Sulfur in Ash from Coal and Coke
D2013 Practice for Preparing Coal Samples for Analysis
D2795 Test Methods for Analysis of Coal and Coke Ash
D3172 Practice for Proximate Analysis of Coal and Coke
D3173 Test Method for Moisture in the Analysis Sample of Coal and Coke
D3176 Practice for Ultimate Analysis of Coal and Coke
D3180 Practice for Calculating Coal and Coke Analyses from As-Determined to Different Bases
D3682 Test Method for Major and Minor Elements in Combustion Residues from Coal Utilization Processes
E691 Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
ICS Number Code 75.160.10 (Solid fuels)
UNSPSC Code 15101601(Coal); 15101604(Coke)