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Work Item

ASTM WK95913

New Test Method for Analyzing Particulate Content of Water for Injection and Clean Pharma Fluids Caused by Spallation of Tubing Used With Peristaltic Pumping Systems

1. Scope
This practice describes a procedure to test laboratory tubing of various plastic tube materials for spallation caused during the pumping of water for injection (WFI) and pharma fluids using a dynamic imaging analyzer (DIA). The range of particle sizes to be detected is 1 µm to 300 µm
Keywords
Particle Counting
Rationale

Without a method to test pump and tube combinations, clean fluids may be contaminated by the process equipment. Referenced standards USP 788 and USP 1788 have very low allowable particulate counts for parenteral fluids. WFI fluids also have similar constraints on particulate maximums. When followed, the test procedure will indicate the level of contamination in a clean fluid that is produced by the interaction of the pump and tubing.

Details

Developed by Subcommittee: E55.14

Committee: E55

Staff Manager: Travis Murdock

Work Item Status

Date Initiated: 08-04-2025

Technical Contact: Ethan Schrodt

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