SYMPOSIA PAPER Published: 01 January 1992

Surface Modification of Austenitic 304 Stainless Steel by N and 11 Ion Implantation


The influence of N2+ and 11B+ ion implantation on the near surface of 304 austenitic stainless steel having strained and strain-free surfaces has been studied. The samples were implanted in a Varian DF-3000 for 3 h at 2 × 10-6 torr with N2+ and 11B+ ions accelerated to an energy of 130 keV at a dose of 2.5 × 1021 ions m-2. The characteristics of the implanted layer and depth profile were investigated by Auger electron spectroscopy (AES) and electron spectroscopy for chemical analysis (ESCA). Scanning electron microscopy was also performed. Relative Knoop hardness numbers were measured at different test loads (19.6 to 490.3 mN). In the mechanically polished samples implanted with N2+ and 11B+ ions, a relative increase of 200 and 30%, respectively, is observed at the 19.6-mN test load. In the case of etched samples implanted with the same ions at the same load, a relative increase of 260 and 80% was observed. Iron nitride and boron nitride precipitates were inferred using ESCA. The increase in near-surface hardness is attributed to the formation of these precipitates and the process of dislocation pinning.

Author Information

Goel, AK
Kurukshetra University, Kurukshetra, India
Sharma, ND
Kurukshetra University, Kurukshetra, India
Mohindra, RK
Kurukshetra University, Kurukshetra, India
Ghosh, PK
University of Roorkee, Roorkee, India
Bhatnagar, MC
Thin Films Lab., Indian Institute of Technology, New Delhi, India
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Developed by Committee: E10
Pages: 1061–1068
DOI: 10.1520/STP17930S
ISBN-EB: 978-0-8031-5187-1
ISBN-13: 978-0-8031-1477-7