Journal Published Online: 01 July 1996
Volume 41, Issue 4

Structural Elucidation of Unusual Police Exhibits. II. Identification and Spectral Characterization of N-(2-Hydroxyethyl)amphetamine Hydrochloride

CODEN: JFSCAS

Abstract

An unusual police exhibit having the physical appearance, color, and odor of methamphetamine hydrochloride was identified unequivocally on the basis of combined evidence from 1H- and 13C-NMR, mass, and infrared spectroscopic examination as N-(2-hydroxyethyl)amphetamine hydrochloride (HEA·HCl). A minor contaminant of the exhibit was similarly identified as ethanolamine hydrochloride (HE·HCl), suggesting synthesis via reductive amination of phenylacetone. Relevant spectroscopic data (1H-, 13C-NMR, mass, and FT-IR) and spectra are presented.

Author Information

Cyr, TD
Bureau of Drug Research, Drugs Directorate, Health Protection Branch, Health Canada
Dawson, BA
Sir F. G. Banting Research Centre, Postal Locator 2201A, Tunney's Pasture, Ottawa, ON, Canada
By, AW
Sir F. G. Banting Research Centre, Postal Locator 2201A, Tunney's Pasture, Ottawa, ON, Canada
Neville, GA
Queen's University, Kingston, ON, Canada
Shurvell, HF
Pages: 4
Price: $25.00
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Stock #: JFS13962J
ISSN: 0022-1198
DOI: 10.1520/JFS13962J