Standard Active Last Updated: Dec 07, 2022 Track Document
ASTM F2328-17(2022)

Standard Test Method for Determining Decarburization and Carburization in Hardened and Tempered Threaded Steel Bolts, Screws, Studs, and Nuts

Standard Test Method for Determining Decarburization and Carburization in Hardened and Tempered Threaded Steel Bolts, Screws, Studs, and Nuts F2328-17R22 ASTM|F2328-17R22|en-US Standard Test Method for Determining Decarburization and Carburization in Hardened and Tempered Threaded Steel Bolts, Screws, Studs, and Nuts Standard new BOS Vol. 01.09 Committee F16
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Significance and Use

4.1 Decarburization and carburization are two surface conditions created, either intentionally or unintentionally, as with a pre-existing condition created during the rod rolling process, the rod/wire annealing process, or while heat treating threaded steel products. Too much of either will adversely affect the safety and performance of the threaded product. Therefore, limits have been established for three different product groups: the harder and greater the tensile strength of the product, the more susceptible to failure the product becomes if these limits are exceeded.

4.2 When testing to a particular product specification that lists the dimensions and microindentation data to be used, that data shall take precedence over the tables in this test method.

4.3 There are only two viable methods available to detect these deficiencies, either by the visual method or the microindentation method. Both methods are used for routine inspections when evaluations are conducted at a single location on the product sample.

4.3.1 Because an evaluation at a specific location may not be representative of the whole part, the referee method employs the microindentation method taken as an average of evaluations conducted on four adjacent threads. This procedure significantly reduces the random test variables when compared to testing on a single thread.

4.4 Specifying this test method does not specify or imply that testing shall be for either decarburization or carburization alone or for both conditions. When either test method is performed, both conditions will be apparent and shall be reported. For example, if an order is placed to test for decarburization and none is found, but the presence of carburization is detected, it shall be reported on the test report that carburization was found.


1.1 This test method covers procedures for measuring, classifying, and determining the presence of decarburization and carburization in the threaded section of hardened and tempered inch series steel bolts, screws, studs, nuts, and similar parts which have been heated to facilitate fabrication or to modify their mechanical properties. This test method is not intended to address products which are intentionally carburized to achieve specific results.

1.2 Two routine methods are described for measuring the limits of and determining the presence of decarburization or carburization—the optical method and the microindentation method 1. Either method is appropriate for routine examinations. The microindentation method 2 shall be considered the referee method.

1.3 For the purpose of these tests, there are four classes of hardened and tempered steel products for which specific measurements must be made with respect to their physical properties.

1.4 The values stated in inch-pound units are to be regarded as standard. No other units of measurement are included in this standard.

1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.

1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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Book of Standards Volume: 01.09
Developed by Subcommittee: F16.01
Pages: 4
DOI: 10.1520/F2328-17R22
ICS Code: 21.060.01; 77.140.20