Standard Historical Last Updated: Dec 31, 2010
ASTM D4590-06

Standard Test Method for Colorimetric Determination of p-tert-Butylcatechol In Styrene Monomer or AMS (alpha-Methylstyrene) by Spectrophotometry

Significance and Use

This test method is suitable for determining the quantity of TBC inhibitor, both for the protection against polymerization while in transit and storage, and for internal quality control.

Scope

1.1 This test method is applicable to the determination of residual 4-tertiary-butylcatechol (TBC) in styrene monomer or AMS in the 1 to 100 ppm range. Any other compound producing color at 490 nm when contacted with aqueous sodium hydroxide solution will interfere. It may be compensated for by including it in the preparation of the standard solutions, if its identity and concentration in the sample are known.

1.2 In determining the conformance of the test results using this method to applicable specifications, results shall be rounded off in accordance with the rounding-off method of Practice E 29.

1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. For specific statements on hazards, see Section 8.

Price:
Contact Sales
Related
Reprints and Permissions
Reprints and copyright permissions can be requested through the
Copyright Clearance Center
Details
Book of Standards Volume: 06.04
Developed by Subcommittee: D16.07
Pages: 3
DOI: 10.1520/D4590-06
ICS Code: 17.180.20; 71.080.60