Standard Active Last Updated: Dec 14, 2017 Track Document
ASTM D3329-03(2017)

Standard Test Method for Purity of Methyl Isobutyl Ketone by Gas Chromatography

Standard Test Method for Purity of Methyl Isobutyl Ketone by Gas Chromatography D3329-03R17 ASTM|D3329-03R17|en-US Standard Test Method for Purity of Methyl Isobutyl Ketone by Gas Chromatography Standard new BOS Vol. 06.04 Committee D01
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Significance and Use

4.1 This test method provides a measurement of commonly found impurities in commercially available methyl isobutyl ketone. The measurement of these impurities and the results thereof can individually or when totaled and subtracted from 100 (assay) be used for specification acceptance.


1.1 This test method covers the determination of the purity of methyl isobutyl ketone (MIBK) by gas chromatography and in addition provides a means for measuring certain impurities such as methyl isobutyl carbinol which are of interest. Impurities such as water and acidity are measured by other appropriate ASTM procedures and the results are used to normalize the chromatographic value.

1.2 The following applies to all specified limits in this standard; for purposes of determining conformance with this standard, an observed value or a calculated value shall be rounded off “to the nearest unit” in the last right-hand digit used in expressing the specification limit, in accordance with the round-off method of Practice E29.

1.3 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.

1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.

1.5 For specific hazard information and guidance, see the supplier’s Safety Data Sheet for the materials listed in this test method.

1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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Book of Standards Volume: 06.04
Developed by Subcommittee: D01.35
Pages: 4
DOI: 10.1520/D3329-03R17
ICS Code: 71.080.80