ASTM F1593 - 08(2016)

    Standard Test Method for Trace Metallic Impurities in Electronic Grade Aluminum by High Mass-Resolution Glow-Discharge Mass Spectrometer

    Active Standard ASTM F1593 | Developed by Subcommittee: F01.17

    Book of Standards Volume: 10.04

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    Significance and Use

    5.1 This test method is intended for application in the semiconductor industry for evaluating the purity of materials (for example, sputtering targets, evaporation sources) used in thin film metallization processes. This test method may be useful in additional applications, not envisioned by the responsible technical committee, as agreed upon by the parties concerned.

    5.2 This test method is intended for use by GDMS analysts in various laboratories for unifying the protocol and parameters for determining trace impurities in pure aluminum. The objective is to improve laboratory to laboratory agreement of analysis data. This test method is also directed to the users of GDMS analyses as an aid to understanding the determination method, and the significance and reliability of reported GDMS data.

    5.3 For most metallic species the detection limit for routine analysis is on the order of 0.01 weight ppm. With special precautions detection limits to sub-ppb levels are possible.

    5.4 This test method may be used as a referee method for producers and users of electronic-grade aluminum materials.

    1. Scope

    1.1 This test method covers measuring the concentrations of trace metallic impurities in high purity aluminum.

    1.2 This test method pertains to analysis by magnetic-sector glow discharge mass spectrometer (GDMS).

    1.3 The aluminum matrix must be 99.9 weight % (3N-grade) pure, or purer, with respect to metallic impurities. There must be no major alloy constituent, for example, silicon or copper, greater than 1000 weight ppm in concentration.

    1.4 This test method does not include all the information needed to complete GDMS analyses. Sophisticated computer-controlled laboratory equipment skillfully used by an experienced operator is required to achieve the required sensitivity. This test method does cover the particular factors (for example, specimen preparation, setting of relative sensitivity factors, determination of sensitivity limits, etc.) known by the responsible technical committee to affect the reliability of high purity aluminum analyses.

    1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

    2. Referenced Documents (purchase separately) The documents listed below are referenced within the subject standard but are not provided as part of the standard.

    ASTM Standards

    E135 Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials

    E177 Practice for Use of the Terms Precision and Bias in ASTM Test Methods

    E691 Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method

    E1257 Guide for Evaluating Grinding Materials Used for Surface Preparation in Spectrochemical Analysis

    ICS Code

    ICS Number Code 77.040.99 (Other methods of testing metals)

    UNSPSC Code

    UNSPSC Code 41115404(Mass spectrometers); 11101705(Aluminum)

    Referencing This Standard
    Link Here
    Link to Active (This link will always route to the current Active version of the standard.)

    DOI: 10.1520/F1593-08R16

    Citation Format

    ASTM F1593-08(2016), Standard Test Method for Trace Metallic Impurities in Electronic Grade Aluminum by High Mass-Resolution Glow-Discharge Mass Spectrometer, ASTM International, West Conshohocken, PA, 2016,

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