ASTM E228 - 17

    Standard Test Method for Linear Thermal Expansion of Solid Materials With a Push-Rod Dilatometer

    Active Standard ASTM E228 | Developed by Subcommittee: E37.05

    Book of Standards Volume: 14.05

      Format Pages Price  
    PDF 10 $45.00   ADD TO CART
    Hardcopy (shipping and handling) 10 $45.00   ADD TO CART
    Standard + Redline PDF Bundle 20 $54.00   ADD TO CART

    Significance and Use

    5.1 Coefficients of linear thermal expansion are required for design purposes and are used, for example, to determine dimensional behavior of structures subject to temperature changes, or thermal stresses that can occur and cause failure of a solid artifact composed of different materials when it is subjected to a temperature excursion.

    5.2 This test method is a reliable method of determining the linear thermal expansion of solid materials.

    5.3 For accurate determinations of thermal expansion, it is absolutely necessary that the dilatometer be calibrated by using a reference material that has a known and reproducible thermal expansion. The appendix contains information relating to reference materials in current general use.

    5.4 The measurement of thermal expansion involves two parameters: change of length and change of temperature, both of them equally important. Neglecting proper and accurate temperature measurement will inevitably result in increased uncertainties in the final data.

    5.5 The test method can be used for research, development, specification acceptance, quality control (QC) and quality assurance (QA).

    1. Scope

    1.1 This test method covers the determination of the linear thermal expansion of rigid solid materials using push-rod dilatometers. This method is applicable over any practical temperature range where a device can be constructed to satisfy the performance requirements set forth in this standard.

    Note 1: Initially, this method was developed for vitreous silica dilatometers operating over a temperature range of –180°C to 900°C. The concepts and principles have been amply documented in the literature to be equally applicable for operating at higher temperatures. The precision and bias of these systems is believed to be of the same order as that for silica systems up to 900°C. However, their precision and bias have not yet been established over the relevant total range of temperature due to the lack of well-characterized reference materials and the need for interlaboratory comparisons.

    1.2 For this purpose, a rigid solid is defined as a material that, at test temperature and under the stresses imposed by instrumentation, has a negligible creep or elastic strain rate, or both, thus insignificantly affecting the precision of thermal-length change measurements. This includes, as examples, metals, ceramics, refractories, glasses, rocks and minerals, graphites, plastics, cements, cured mortars, woods, and a variety of composites.

    1.3 The precision of this comparative test method is higher than that of other push-rod dilatometry techniques (for example, Test Method D696) and thermomechanical analysis (for example, Test Method E831) but is significantly lower than that of absolute methods such as interferometry (for example, Test Method E289). It is generally applicable to materials having absolute linear expansion coefficients exceeding 0.5 μm/(m·°C) for a 1000°C range, and under special circumstances can be used for lower expansion materials when special precautions are used to ensure that the produced expansion of the specimen falls within the capabilities of the measuring system. In such cases, a sufficiently long specimen was found to meet the specification.

    1.4 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

    1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

    1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

    2. Referenced Documents (purchase separately) The documents listed below are referenced within the subject standard but are not provided as part of the standard.

    ASTM Standards

    D696 Test Method for Coefficient of Linear Thermal Expansion of Plastics Between 30C and 30C with a Vitreous Silica Dilatometer

    E220 Test Method for Calibration of Thermocouples By Comparison Techniques

    E289 Test Method for Linear Thermal Expansion of Rigid Solids with Interferometry

    E473 Terminology Relating to Thermal Analysis and Rheology

    E644 Test Methods for Testing Industrial Resistance Thermometers

    E831 Test Method for Linear Thermal Expansion of Solid Materials by Thermomechanical Analysis

    E1142 Terminology Relating to Thermophysical Properties

    ICS Code

    ICS Number Code 77.040.99 (Other methods of testing of metals)

    UNSPSC Code

    UNSPSC Code

    Referencing This Standard
    Link Here
    Link to Active (This link will always route to the current Active version of the standard.)

    DOI: 10.1520/E0228-17

    Citation Format

    ASTM E228-17, Standard Test Method for Linear Thermal Expansion of Solid Materials With a Push-Rod Dilatometer, ASTM International, West Conshohocken, PA, 2017,

    Back to Top