ASTM E1645 - 16

    Standard Practice for Preparation of Dried Paint Samples by Hotplate or Microwave Digestion for Subsequent Lead Analysis

    Active Standard ASTM E1645 | Developed by Subcommittee: D22.12

    Book of Standards Volume: 11.07

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    Significance and Use

    5.1 Paint in buildings and related structures needs to be monitored for lead content in order to determine the potential lead hazard. Hence, effective and efficient methods are required for the preparation of paint samples that may contain lead.

    5.2 This practice may be used for the digestion of paint samples that are collected during various lead-hazard control and risk assessment activities associated with lead abatement in and around buildings and related structures. This practice is also suitable for the digestion of paint samples collected from locations such as commercial buildings.

    5.3 This practice may be used to prepare samples that have been obtained in order to ensure compliance with laws that govern lead content in paints.

    5.4 This practice may be used to prepare samples that have been collected for risk assessment purposes.

    5.5 This practice is intended for use with paint samples that are prepared for subsequent analysis by quantitative analytical methods.

    1. Scope

    1.1 This practice covers the sample preparation procedures for paint samples that are collected during the assessment, management or control of lead hazards.

    1.2 This practice describes the digestion procedures using a hot plate or microwave oven or apparatus for paint samples that are to be analyzed for lead content.

    1.3 This practice covers the general considerations for quantitative sample extraction for total recoverable lead in dried paint samples (either bulk paint or paint powder) using hot plate or microwave heating techniques, or both.

    1.4 This practice contains notes that are explanatory and not part of the mandatory requirements of the standard.

    1.5 This practice is based on two NIOSH Methods, 7082 and 7105, and on an EPA standard operating procedure for lead in paint.

    1.6 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

    1.7 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. For specific warning statements, see 6.1.2,,,, 7.2.1, and 7.2.2.

    2. Referenced Documents (purchase separately) The documents listed below are referenced within the subject standard but are not provided as part of the standard.

    ISO Documents

    ISO 1042 Laboratory glassware -- One-mark volumetric flasks

    ISO 8655

    ISO Guide 30 Reference materials -- Selected terms and definitions

    ASTM Standards

    D1129 Terminology Relating to Water

    D1193 Specification for Reagent Water

    E288 Specification for Laboratory Glass Volumetric Flasks

    E969 Specification for Glass Volumetric (Transfer) Pipets

    E1605 Terminology Relating to Lead in Buildings


    Other Documents

    NMAM 7082 and7105 NIOSH Manual of Analytical Methods, 4th ed.

    NTIS No. PB92–114172 Standard Operating Procedures for Lead in Paint by Hotplate- or Microwave-based Acid Digestions and Atomic Absorption or Inductively Coupled Plasma Emission Spectrometry

    ICS Code

    ICS Number Code 87.040 (Paints and varnishes)

    UNSPSC Code

    UNSPSC Code 31211500(Paints and primers)

    Referencing This Standard
    Link Here
    Link to Active (This link will always route to the current Active version of the standard.)

    DOI: 10.1520/E1645-16

    Citation Format

    ASTM E1645-16, Standard Practice for Preparation of Dried Paint Samples by Hotplate or Microwave Digestion for Subsequent Lead Analysis, ASTM International, West Conshohocken, PA, 2016,

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