ASTM E1545 - 11(2016)

    Standard Test Method for Assignment of the Glass Transition Temperature by Thermomechanical Analysis

    Active Standard ASTM E1545 | Developed by Subcommittee: E37.10

    Book of Standards Volume: 14.05

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    Significance and Use

    5.1 The glass transition is dependent on the thermal history of the material to be tested. For amorphous and semicrystalline materials the assignment of the glass transition temperature may lead to important information about thermal history, processing conditions, stability, progress of chemical reactions, and mechanical and electrical behavior.

    5.2 Thermomechanical analysis provides a rapid means of detecting changes in hardness or linear expansion associated with the glass transition.

    5.3 This test method is useful for research and development, quality control, and specification acceptance.

    1. Scope

    1.1 This test method describes procedures for the assignment of the glass transition temperature of materials on heating using thermomechanical measurements under compression experimental conditions.

    1.2 This test method is applicable to amorphous or to partially crystalline materials that are sufficiently rigid below the glass transition to inhibit indentation by the sensing probe.

    1.3 The normal operating temperature range is from − 100 to 600°C. This temperature range may be extended depending upon the instrumentation used.

    1.4 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

    1.5 This test method is related to ISO 11359-2. ISO 11359-2 additionally covers the determination of coefficient of linear thermal expansion not covered by this test method. This test method is related to IEC 61006 but uses a slower heating rate.

    1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Specific precautionary statements are given in Section 7.

    2. Referenced Documents (purchase separately) The documents listed below are referenced within the subject standard but are not provided as part of the standard.

    ASTM Standards

    E473 Terminology Relating to Thermal Analysis and Rheology

    E691 Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method

    E1142 Terminology Relating to Thermophysical Properties

    E1363 Test Method for Temperature Calibration of Thermomechanical Analyzers

    Other Standards

    ISO 11359-2 PlasticsThermomechanical Analysis (TMA) Part 2: Determination of Coefficient of Linear Thermal Expansion and Glass Transition Temperature Available from American National Standards Institute (ANSI), 25 W. 43rd St., 4th Floor, New York, NY 10036,

    ICS Code

    ICS Number Code 81.040.01 (Glass in general)

    Referencing This Standard
    Link Here
    Link to Active (This link will always route to the current Active version of the standard.)

    DOI: 10.1520/E1545-11R16

    Citation Format

    ASTM E1545-11(2016), Standard Test Method for Assignment of the Glass Transition Temperature by Thermomechanical Analysis, ASTM International, West Conshohocken, PA, 2016,

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