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    ASTM D8186 - 18

    Standard Test Method for Measurement of Impurities in Graphite by Electrothermal Vaporization Inductively Coupled Plasma Optical Emission Spectrometry (ETV-ICP OES)

    Active Standard ASTM D8186 | Developed by Subcommittee: D02.F0

    Book of Standards Volume: 05.05

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    Significance and Use

    5.1 The presence and content of various impurities in graphite are major considerations in determining the suitability of graphite for various applications. This test method provides an alternative means of determining the content of trace impurities in a graphite sample which has considerable advantages compared to classical wet-chemical analysis methods.

    5.2 The test method provides a standard procedure to measure impurities in graphite and to assure required graphite specifications.

    1. Scope

    1.1 This test method covers the measurement of mass fractions of the elements silver (Ag), aluminum (Al), arsenic (As), boron (B), barium (Ba), berylium (Be), bismuth (Bi), calcium (Ca), cadmium (Cd), cobalt (Co), chromium (Cr), copper (Cu), iron (Fe), potassium (K), lithium (Li), magnesium (Mg), manganese (Mn), molybdenum (Mo), sodium (Na), nickel (Ni), phosphorus (P), lead (Pb), sulfur (S), antimony (Sb), silicon (Si), tin (Sn), strontium (Sr), titanium (Ti), vanadium (V), tungsten (W), yitrium (Y), zinc (Zn), and zirconium (Zr) in graphite.

    1.2 Provided that an appropriate validation procedure is carried out, this test method is also applicable to other carbon materials such as coal, coke, carbon black, graphite-felt, graphite-foil, graphite-foam, and fiber reinforced carbon-carbon composites.

    1.3 This test method is applicable to element contents from approximately 0.0001 mg/kg to 1000 mg/kg (0.1 ppmw to 1000 ppmw), depending on element, wavelength, measurement parameters, and sample mass.

    1.4 The values stated in SI units are to be regarded as standard. The values given in parentheses after SI units are provided for information only and are not considered standard.

    1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.

    1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

    2. Referenced Documents (purchase separately) The documents listed below are referenced within the subject standard but are not provided as part of the standard.

    ASTM Standards

    D1193 Specification for Reagent Water

    ISO Standards

    ISO 5725-2 Accuracy (trueness and precision) of measurement methods and resultsPart 2: Basic method for the determination of repeatability and reproducibility of a standard measurement method

    ICS Code

    ICS Number Code 71.060.10 (Chemical elements)

    UNSPSC Code

    UNSPSC Code 11101507(Graphite)

    Referencing This Standard
    Link Here
    Link to Active (This link will always route to the current Active version of the standard.)

    DOI: 10.1520/D8186-18

    Citation Format

    ASTM D8186-18, Standard Test Method for Measurement of Impurities in Graphite by Electrothermal Vaporization Inductively Coupled Plasma Optical Emission Spectrometry (ETV-ICP OES), ASTM International, West Conshohocken, PA, 2018, www.astm.org

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