ASTM D8088 - 16
Standard Practice for Determination of the Six Major Rare Earth Elements in Fluid Catalytic Cracking Catalysts, Zeolites, Additives, and Related Materials by Inductively Coupled Plasma Optical Emission Spectroscopy
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Significance and Use
5.1 The chemical composition of catalysts and catalyst materials is an important indicator of catalyst performance and is a valuable tool for assessing parameters in a FCCU process. This practice will be useful to catalyst manufacturers and petroleum refiners for quality verification and performance evaluation, and to environmental authorities at the state and federal levels for evaluation and verification of various compliance programs (1, 2, 3).
1. Scope
1.1 This practice describes the analysis of fluid catalytic cracking catalysts, rare earth exchanged zeolitic materials, additive and related materials when analyzed by ICP-OES for the six most common rare earth elements.
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this Practice.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. See Appendix X3.
2. Referenced Documents (purchase separately) The documents listed below are referenced within the subject standard but are not provided as part of the standard.
ASTM Standards
C1109 Practice for Analysis of Aqueous Leachates from Nuclear Waste Materials Using Inductively Coupled Plasma-Atomic Emission Spectroscopy
D1193 Specification for Reagent Water
D3766 Terminology Relating to Catalysts and Catalysis
D6299 Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
D6349 Test Method for Determination of Major and Minor Elements in Coal, Coke, and Solid Residues from Combustion of Coal and Coke by Inductively Coupled Plasma--Atomic Emission Spectrometry
D7085 Guide for Determination of Chemical Elements in Fluid Catalytic Cracking Catalysts by X-ray Fluorescence Spectrometry (XRF)
D7260 Practice for Optimization, Calibration, and Validation of Inductively Coupled Plasma-Atomic Emission Spectrometry (ICP-AES) for Elemental Analysis of Petroleum Products and Lubricants
D7442 Practice for Sample Preparation of Fluid Catalytic Cracking Catalysts and Zeolites for Elemental Analysis by Inductively Coupled Plasma Optical Emission Spectroscopy
E1479 Practice for Describing and Specifying Inductively-Coupled Plasma Atomic Emission Spectrometers
EPA Standard
Method 6010B Inductively Coupled Plasma-Atomic Emission SpectrometryICS Code
ICS Number Code 77.040.20 (Non-destructive testing of metals)
UNSPSC Code
UNSPSC Code 12161604(Cracking catalysts)
Referencing This Standard
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DOI: 10.1520/D8088-16
Citation Format
ASTM D8088-16, Standard Practice for Determination of the Six Major Rare Earth Elements in Fluid Catalytic Cracking Catalysts, Zeolites, Additives, and Related Materials by Inductively Coupled Plasma Optical Emission Spectroscopy, ASTM International, West Conshohocken, PA, 2016, www.astm.org
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