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    ASTM D7997 - 21

    Standard Practice for Polyurethane Raw Materials: Gel Tests for Polyurethane Non-Foam Formulations

    Active Standard ASTM D7997 | Developed by Subcommittee: D20.22

    Book of Standards Volume: 08.03

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    Significance and Use

    5.1 General Utility: 

    5.1.1 This practice is suitable for research, quality control, specification testing and process control.

    5.1.2 It is useful to define and verify the reactivity of non-foam polyurethane formulations.

    5.2 Limitations: 

    5.2.1 Operator-to-operator variability and lab-to-lab variability can be significant.

    5.2.2 The variability of this practice is dependent on the equipment used to measure the gel time. It is recommended that the testing laboratory and the client agree on the equipment and the conditions to be used that include the following: Gel Tester and gel point criteria, Speed/rpm of the mixer, Type and shape of the mix blades, Size and type (for example, shape, lined or unlined) of container for mixing the components and for measuring the gel time, and The volume (or height) of material to be placed in the container for measuring the gel time and the depth of the measuring wire or spindle of the gel tester from the bottom of the container.

    5.2.3 Users of this practice shall develop their own precision data to determine if these procedures meet their requirements.

    5.2.4 It is possible that low-levels (ppm, ppb) of contaminants will not be detected using this practice.

    1. Scope

    1.1 This practice covers procedures for determining the gel times of polyurethane non-foam formulations using commercially available gel test equipment.

    1.2 Definitions, terms, and techniques are described along with procedures for calculating sample weights.

    1.3 The values stated in SI units are to be regarded as standard.

    1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.

    Note 1: There is no known ISO equivalent to this standard.

    1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

    2. Referenced Documents (purchase separately) The documents listed below are referenced within the subject standard but are not provided as part of the standard.

    ASTM Standards

    D883 Terminology Relating to Plastics

    ICS Code

    ICS Number Code 83.080.10 (Thermosetting materials)

    UNSPSC Code

    UNSPSC Code 13111300(Foams); 13111061(Polyurethane resins)

    Referencing This Standard
    Link Here
    Link to Active (This link will always route to the current Active version of the standard.)

    DOI: 10.1520/D7997-21

    Citation Format

    ASTM D7997-21, Standard Practice for Polyurethane Raw Materials: Gel Tests for Polyurethane Non-Foam Formulations, ASTM International, West Conshohocken, PA, 2021, www.astm.org

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