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Significance and Use
5.1 Respirable crystalline silica is a hazard to the health of workers in many industries who are at risk through exposure by inhalation. Industrial hygienists and other public health professionals need to determine the effectiveness of measures taken to control workers’ exposure, and this is generally achieved by taking workplace air measurements. This standard has been published in order to make available a method for making valid exposure measurements for crystalline silica exposures in industry. It will be of benefit to: agencies concerned with health and safety at work; industrial hygienists and other public health professionals; analytical laboratories; industrial users of silica-containing products and their workers, etc.
5.2 This standard specifies a generic sampling and analytical method for measurement of the mass concentration of respirable crystalline silica in workplace air using infrared (IR) spectrometric methods. Several different types of sampling apparatus are used to collect respirable dust, according to the occupational hygiene sampling convention. This standard is designed to accommodate a variety of appropriate samplers and sampling materials that are commercially available.
1.1 This standard specifies a test method for collection and analysis of samples of airborne particulate matter for measurement of respirable crystalline silica by infrared (IR) spectrometry.
1.2 This test method is applicable to the analysis of crystalline silica (the polymorphs quartz, cristobalite and tridymite) over a working range of 0.025 to 0.4 mg/m3 for a 400 L air sample or 0.02 to 0.25 mg/m3 for a 1000 L air sample, depending on the analytical method.
1.3 The methodology is applicable to personal sampling of the respirable fraction of airborne particles and to static (area) sampling.
1.4 This test method describes three different procedures for sample preparation and infrared analysis of airborne crystalline silica samples, which are delineated in , respectively: (1) a potassium bromide (KBr) disc IR measurement method, (2) indirect IR analysis after redeposition onto a filter used for measurement, and (3) direct on-filter IR analysis.
1.5 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
2. Referenced Documents (purchase separately) The documents listed below are referenced within the subject standard but are not provided as part of the standard.
D1356 Terminology Relating to Sampling and Analysis of Atmospheres
D4532 Test Method for Respirable Dust in Workplace Atmospheres Using Cyclone Samplers
D4840 Guide for Sample Chain-of-Custody Procedures
D5337 Practice for Flow Rate Adjustment of Personal Sampling Pumps
D6061 Practice for Evaluating the Performance of Respirable Aerosol Samplers
E1370 Guide for Air Sampling Strategies for Worker and Workplace Protection
ISO StandardsISO 13137 ISO 15767 Workplace atmospheres Controlling and characterizing errors in weighing collected aerosols ISO 18158 Workplace air Terminology ISO 24095 ISO 7708 Air quality Particle size fraction definitions for health-related sampling ISO/IEC 17025
ICS Number Code 13.040.30 (Workplace atmospheres)
UNSPSC Code 77121501(Air quality management)
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ASTM D7948-20, Standard Test Method for Measurement of Respirable Crystalline Silica in Workplace Air by Infrared Spectrometry, ASTM International, West Conshohocken, PA, 2020, www.astm.orgBack to Top