ASTM D7344 - 17

    Standard Test Method for Distillation of Petroleum Products and Liquid Fuels at Atmospheric Pressure (Mini Method)

    Active Standard ASTM D7344 | Developed by Subcommittee: D02.08

    Book of Standards Volume: 05.04

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    Significance and Use

    5.1 The distillation (volatility) characteristics of hydrocarbons and other liquids have an important effect on their safety and performance, especially in the case of fuels and solvents. The boiling range gives information on the composition, the properties, and the behavior of the fuel during storage and use. Volatility is the major determinant of the tendency of a hydrocarbon mixture to produce potentially explosive vapors.

    5.2 The distillation characteristics are equally important for both automotive and aviation gasolines, affecting starting, warm-up, and tendency to vapor lock at high operating temperatures or high altitude, or both. The presence of high boiling point components in these and other fuels can significantly affect the degree of formation of solid combustion deposits.

    5.3 Volatility, as it affects the rate of evaporation, is an important factor in the application of many solvents, particularly those used in paints.

    5.4 Distillation limits are often included in petroleum product specifications, in commercial contract agreements, process refinery/control applications, and for compliance to regulatory rules.

    5.5 This test method is suitable for setting specifications, for use as an internal quality control tool, and for use in development or research work on hydrocarbon solvents.

    5.5.1 This test method gives a broad indication of general purity and can also indicate presence of excessive moisture. It will not differentiate between products of similar boiling range.

    1. Scope

    1.1 This test method covers the procedure for the determination of the distillation characteristics of petroleum products and liquid fuels in the range of 20 °C to 400 °C (68 °F to 752 °F) using miniaturized automatic distillation apparatus.

    1.2 This test method is applicable to such products as: light and middle distillates, automotive spark-ignition engine fuels, automotive spark-ignition engine fuels containing up to 10 % ethanol, aviation gasolines, aviation turbine fuels, all grades of No. 1 and No. 2 diesel fuels (as described in Specification D975), biodiesel (B100), biodiesel blends up to 30 % biodiesel, special petroleum spirits, pure petrochemical compounds, naphthas, white spirits, kerosenes, furnace fuel oils, and distillate marine fuels.

    Note 1: The up to 10 % by volume ethanol limit in spark ignition engine fuels (E10) was the range used in the supporting interlaboratory studies. Spark ignition engine fuels containing > 10 % by volume ethanol and up to 20 % by volume ethanol (E20) may be analyzed, however the stated precision and bias does not apply.

    1.3 This test method is designed for the analysis of distillate products; it is not applicable to products containing appreciable quantities of residual material.

    1.4 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.

    1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

    1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

    2. Referenced Documents (purchase separately) The documents listed below are referenced within the subject standard but are not provided as part of the standard.

    ASTM Standards

    D86 Test Method for Distillation of Petroleum Products and Liquid Fuels at Atmospheric Pressure

    D323 Test Method for Vapor Pressure of Petroleum Products (Reid Method)

    D975 Specification for Diesel Fuel Oils

    D1160 Test Method for Distillation of Petroleum Products at Reduced Pressure

    D4057 Practice for Manual Sampling of Petroleum and Petroleum Products

    D4177 Practice for Automatic Sampling of Petroleum and Petroleum Products

    D4953 Test Method for Vapor Pressure of Gasoline and Gasoline-Oxygenate Blends (Dry Method)

    D5190 Test Method for Vapor Pressure of Petroleum Products (Automatic Method)

    D5191 Test Method for Vapor Pressure of Petroleum Products (Mini Method)

    D5482 Test Method for Vapor Pressure of Petroleum Products (Mini Method--Atmospheric)

    D6300 Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants

    D6708 Practice for Statistical Assessment and Improvement of Expected Agreement Between Two Test Methods that Purport to Measure the Same Property of a Material

    Energy Institute Standards

    IP 394 Determination of Air Saturated Vapour Pressure

    IP 69 Determination of Vapour PressureReid Method

    ICS Code

    ICS Number Code 75.180.20 (Processing equipment)

    UNSPSC Code

    UNSPSC Code 15101500(Petroleum and distillates)

    Referencing This Standard
    Link Here
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    DOI: 10.1520/D7344-17

    Citation Format

    ASTM D7344-17, Standard Test Method for Distillation of Petroleum Products and Liquid Fuels at Atmospheric Pressure (Mini Method), ASTM International, West Conshohocken, PA, 2017,

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