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    ASTM D7200-12

    Standard Practice for Sampling and Counting Airborne Fibers, Including Asbestos Fibers, in Mines and Quarries, by Phase Contrast Microscopy and Transmission Electron Microscopy (Withdrawn 2021)

    Withdrawn Standard: ASTM D7200-12 | Developed by Subcommittee: D22.07


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    Withdrawn Rationale:

    This practice describes the determination of the concentration of fibers, expressed as the number of such fibers per millilitre of air, using phase contrast microscopy and optionally transmission electron microscopy to evaluate particulate material collected on a membrane filter in the breathing zone of an individual or by area sampling in a specific location.

    Formerly under the jurisdiction of Committee D22 on Air Quality, this practice was withdrawn in January 2021 in accordance with section 10.6.3 of the Regulations Governing ASTM Technical Committees, which requires that standards shall be updated by the end of the eighth year since the last approval date.

    1. Scope

    1.1 This practice2 describes the determination of the concentration of fibers, expressed as the number of such fibers per millilitre of air, using phase contrast microscopy and optionally transmission electron microscopy to evaluate particulate material collected on a membrane filter in the breathing zone of an individual or by area sampling in a specific location. This practice is based on the core procedures provided in the International Organization for Standardization (ISO) Standard ISO 8672(1)3, the National Institute for Occupational and Health (NIOSH) Manual of Analytical Methods, NIOSH 7400 (2), and the Occupational Safety and Health Administration (OSHA) Method ID 160 (3). This practice indicates the important points where these methods differ, and provides information regarding the differences. However, selecting portions of procedures from different published methods generally requires a user to report that they have used a modification to a method rather than claim they have used the method as written. This practice further gives guidance on how differential counting techniques may be used to indicate where a population of fibers may be asbestos.

    1.2 The practice is used for routine determination of an index of occupational exposure to airborne fibers in mines, quarries, or other locations where ore may be processed or handled. The method gives an index of airborne fiber concentration. The method provides an estimate of the fraction of counted fibers that may be asbestos. This practice should be used in conjunction with electron microscopy (See Appendix X1) for assistance in identification of fibers.

    1.3 This practice specifies the equipment and procedures for sampling the atmosphere in the breathing zone of an individual and for determining the number of fibers accumulated on a filter membrane during the course of an appropriately-selected sampling period. The method may also be used to sample the atmosphere in a specific location in a mine or in a room of a building (area sampling).

    1.4 The ideal working range of this practice extends from 100 fibers/mm2 to 1300 fibers/mm2 of filter area. For a 1000-L air sample, this corresponds to a concentration range from approximately 0.04 to 0.5 fiber/mL (or fiber/cm3). Lower and higher ranges of fiber concentration can be measured by reducing or increasing the volume of air collected. However, when this practice is applied to personal sampling in mines and quarries, the level of total suspended particulate may impose an upper limit to the volume of air that can be sampled if the filters produced are to be of appropriate particulate loading for fiber counting.

    1.5 Users should determine their own limit of detection using the procedure in Practice D6620. For reference, the NIOSH 7400 method gives the limit of detection as 7 fibers/mm2 of filter area. For a 1000-L air sample, this corresponds to a limit of detection of 0.0027 fiber/mL (or fiber/cm3). For OSHA ID 160 the limit of detection is given as 5.5 fibers/mm2 of filter area. For a 1000-L air sample, this corresponds to a limit of detection of 0.0022 fiber/mL (or fiber/cm3).

    1.6 If this practice yields a fiber concentration that does not exceed one-half the permissible exposure limit or threshold limit value for the particular regulated fiber variety, no further action may be necessary. If the fiber concentration exceeds one-half of the regulated permissible exposure limit or threshold limit value for the particular regulated fiber variety, it is necessary to examine the data to determine if more than 50 % of the counted fibers are thinner than 1.0 μm, or thicker but with an appearance of asbestos (curvature, splayed ends, or the appearance of a bundle).

    1.7 The mounting medium used in this practice has a refractive index of approximately 1.45. Fibers with refractive indices in the range of 1.4 to 1.5 will exhibit reduced contrast, and may be difficult to detect.

    1.8 Fibers less than approximately 0.2 µm in diameter may not be detected by this practice. (4)

    1.9 This standard may involve hazardous materials, operations, and equipment. This standard does not purport to address all of the safety problems associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. For specific precautionary statements, see Section 7.



    2. Referenced Documents (purchase separately) The documents listed below are referenced within the subject standard but are not provided as part of the standard.

    ASTM Standards

    D257 Test Methods for DC Resistance or Conductance of Insulating Materials

    D1356 Terminology Relating to Sampling and Analysis of Atmospheres

    D1357 Practice for Planning the Sampling of the Ambient Atmosphere

    D3670 Guide for Determination of Precision and Bias of Methods of Committee D22

    D5337 Practice for Flow Rate Adjustment of Personal Sampling Pumps

    D6281 Test Method for Airborne Asbestos Concentration in Ambient and Indoor Atmospheres as Determined by Transmission Electron Microscopy Direct Transfer (TEM)

    D6620 Practice for Asbestos Detection Limit Based on Counts

    Other Standards

    ID160 Occupational Safety and Health Administration (OSHA)

    ISO8672 International Organization for Standardization

    NIOSH 7400 National Institute of Occupational Health and Safety (Revised 1994) This standard is available from US Department of Health and Human Services, 4676 Columbia Parkway, Cincinnati, OH 45226.

    Other Documents

    ISO10312 () This Appendix is based on NIOSH Method 7402 and ISO10312. These methods have different definitions of countable fibers. The minimum diameter for NIOSH Method 7402 is 0.25 m while that for ISO10312 is 0.2 m. NIOSH Method 7402 has no upper limit on fiber width, while that for ISO10312 is 3.0 m. The ISO definition has been used in the text, but the NIOSH definition may be substituted.

    NIOSH Method 7402


    Referencing This Standard
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    DOI: 10.1520/D7200-12

    Citation Format

    ASTM D7200-12, Standard Practice for Sampling and Counting Airborne Fibers, Including Asbestos Fibers, in Mines and Quarries, by Phase Contrast Microscopy and Transmission Electron Microscopy (Withdrawn 2021), ASTM International, West Conshohocken, PA, 2012, www.astm.org

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