ASTM D6969 - 17
Standard Practice for Preparation of Calcined Petroleum Coke Samples for Analysis
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Significance and Use
4.1 This practice provides field personnel and laboratories with standard procedures for dividing, reducing, and mixing gross samples and intermediate samples, such that the resulting prepared analysis samples are more uniform from laboratory to laboratory. Adherence to these guidelines is expected to provide significant reduction in interlaboratory variability.
1. Scope
1.1 This practice covers the preparation procedures necessary for the reduction and division of calcined petroleum coke samples in order to generate appropriate analytical samples upon which physical and chemical analytical tests will be performed.
1.2 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in non-conformance with the standard.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
2. Referenced Documents (purchase separately) The documents listed below are referenced within the subject standard but are not provided as part of the standard.
ASTM Standards
D1552 Test Method for Sulfur in Petroleum Products by High Temperature Combustion and Infrared (IR) Detection or Thermal Conductivity Detection (TCD)
D2638 Test Method for Real Density of Calcined Petroleum Coke by Helium Pycnometer
D4292 Test Method for Determination of Vibrated Bulk Density of Calcined Petroleum Coke
D4422 Test Method for Ash in Analysis of Petroleum Coke
D4930 Test Method for Dust Control Material on Calcined Petroleum Coke
D4931 Test Method for Gross Moisture in Green Petroleum Coke
D5004 Test Method for Real Density of Calcined Petroleum Coke by Xylene Displacement
D5056 Test Method for Trace Metals in Petroleum Coke by Atomic Absorption
D5187 Test Method for Determination of Crystallite Size (Lc) of Calcined Petroleum Coke by X-Ray Diffraction
D5600 Test Method for Trace Metals in Petroleum Coke by Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES)
D5709 Test Method for Sieve Analysis of Petroleum Coke
D6376 Test Method for Determination of Trace Metals in Petroleum Coke by Wavelength Dispersive X-ray Fluorescence Spectroscopy
D7454 Test Method for Determination of Vibrated Bulk Density of Calcined Petroleum Coke using a Semi-Automated Apparatus
ICS Code
ICS Number Code 75.160.10 (Solid fuels)
Referencing This Standard
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DOI: 10.1520/D6969-17
Citation Format
ASTM D6969-17, Standard Practice for Preparation of Calcined Petroleum Coke Samples for Analysis, ASTM International, West Conshohocken, PA, 2017, www.astm.org
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