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Significance and Use
5.1 Gasoline-range olefinic hydrocarbons have been demonstrated to contribute to photochemical reactions in the atmosphere, which result in the formation of photochemical smog in susceptible urban areas.
5.2 The California Air Resources Board (CARB) has specified a maximum allowable limit of total olefins in motor gasoline. This necessitates an appropriate analytical test method for determination of total olefins to be used both by regulators and producers.
5.3 This test method compares favorably with Test Method (FIA) for the determination of total olefins in motor gasolines. It does not require any sample preparation, has a comparatively short analysis time of about 10 min, and is readily automated. Alternative methods for determination of olefins in gasoline include Test Methods and .
1.1 This test method covers the determination of the total amount of olefins in blended motor gasolines and gasoline blending stocks by supercritical-fluid chromatography (SFC). Results are expressed in terms of mass percent olefins. The method working range is from expected concentration of 1 % by mass to expected concentration of 25 % by mass total olefins.
1.2 This test method can be used for analysis of commercial gasolines, including those containing varying levels of oxygenates, such as methyl tert/butyl ether (MTBE), diisopropyl ether (DIPE), methyl tert/amyl ether (TAME), and ethanol, without interference.
Note 1: This test method has not been designed for the determination of the total amounts of saturates, aromatics, and oxygenates.
1.3 This test method includes a relative bias section based on Practice accuracy assessment between Test Method mass percent and Test Method volume percent for total olefins in spark-ignition engine fuels as a possible Test Method alternative to Test Method for U.S. EPA regulations reporting. The Practice derived correlation equation is only applicable for test result range from 0.53 % to 26.88 % by mass as reported by Test Method .
1.4 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
2. Referenced Documents (purchase separately) The documents listed below are referenced within the subject standard but are not provided as part of the standard.
D1319 Test Method for Hydrocarbon Types in Liquid Petroleum Products by Fluorescent Indicator Adsorption
D4052 Test Method for Density, Relative Density, and API Gravity of Liquids by Digital Density Meter
D5186 Test Method for Determination of the Aromatic Content and Polynuclear Aromatic Content of Diesel Fuels By Supercritical Fluid Chromatography
D6296 Test Method for Total Olefins in Spark-ignition Engine Fuels by Multidimensional Gas Chromatography
D6299 Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
D6300 Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products, Liquid Fuels, and Lubricants
D6708 Practice for Statistical Assessment and Improvement of Expected Agreement Between Two Test Methods that Purport to Measure the Same Property of a Material
D6839 Test Method for Hydrocarbon Types, Oxygenated Compounds, and Benzene in Spark Ignition Engine Fuels by Gas Chromatography
ICS Number Code 27.060.10 (Liquid and solid fuel burners)
UNSPSC Code 15101506(Gasoline or Petrol)
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ASTM D6550-20, Standard Test Method for Determination of Olefin Content of Gasolines by Supercritical-Fluid Chromatography, ASTM International, West Conshohocken, PA, 2020, www.astm.orgBack to Top