ASTM D6334 - 12(2017)e1
Standard Test Method for Sulfur in Gasoline by Wavelength Dispersive X-Ray Fluorescence
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Significance and Use
4.1 Knowledge of the presence of sulfur in petroleum products, especially fuels, helps predict performance characteristics, potential corrosion problems, and vehicle emission levels. In addition, some regulatory agencies mandate reduced levels of sulfur in reformulated type gasolines.
1. Scope
1.1 This test method covers the quantitative determination of total sulfur in gasoline and gasoline-oxygenate blends. The Pooled Limit of Quantitation (PLOQ) was determined to be 15 mg/kg. Therefore, the practical range for this test method is from 15 mg/kg to 940 mg/kg.
Note 1: This concentration range is based on that used in the interlaboratory round robin, which shows that the range of sulfur in the round robin samples was from 1.5 mg/kg to 940 mg/kg; however, below 15 mg/kg, the reproducibility approaches 100 % of the concentration.
1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.3 The values stated in SI units are to be regarded as the standard. The preferred units are mg/kg sulfur.
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
2. Referenced Documents (purchase separately) The documents listed below are referenced within the subject standard but are not provided as part of the standard.
ASTM Standards
D2622 Test Method for Sulfur in Petroleum Products by Wavelength Dispersive X-ray Fluorescence Spectrometry
D3210 Test Method for Comparing Colors of Films from Water-Emulsion Floor Polishes
D4045 Test Method for Sulfur in Petroleum Products by Hydrogenolysis and Rateometric Colorimetry
D4057 Practice for Manual Sampling of Petroleum and Petroleum Products
D4177 Practice for Automatic Sampling of Petroleum and Petroleum Products
D4294 Test Method for Sulfur in Petroleum and Petroleum Products by Energy Dispersive X-ray Fluorescence Spectrometry
D5453 Test Method for Determination of Total Sulfur in Light Hydrocarbons, Spark Ignition Engine Fuel, Diesel Engine Fuel, and Engine Oil by Ultraviolet Fluorescence
D5842 Practice for Sampling and Handling of Fuels for Volatility Measurement
D5854 Practice for Mixing and Handling of Liquid Samples of Petroleum and Petroleum Products
D6299 Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance
D6792 Practice for Quality Management Systems in Petroleum Products, Liquid Fuels, and Lubricants Testing Laboratories
ICS Code
ICS Number Code 71.040.50 (Physicochemical methods of analysis); 75.160.20 (Liquid fuels)
UNSPSC Code
UNSPSC Code 15101506(Gasoline or Petrol)
Referencing This Standard
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DOI: 10.1520/D6334-12R17E01
Citation Format
ASTM D6334-12(2017)e1, Standard Test Method for Sulfur in Gasoline by Wavelength Dispersive X-Ray Fluorescence, ASTM International, West Conshohocken, PA, 2017, www.astm.org
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