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    ASTM D5756-02(2008)

    Standard Test Method for Microvacuum Sampling and Indirect Analysis of Dust by Transmission Electron Microscopy for Asbestos Mass Surface Loading (Withdrawn 2017)

    Withdrawn Standard: ASTM D5756-02(2008) | Developed by Subcommittee: D22.07


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    Withdrawn Rationale:

    This test method covers a procedure to (a) identify asbestos in dust and (b) provide an estimate of the surface loading of asbestos in the sampled dust, reported as either the mass of asbestos per unit area of sampled surface or as the mass of asbestos per mass of sampled dust.

    Formerly under the jurisdiction of Committee D22 on Air Quality, this test method was withdrawn in January 2017 in accordance with section 10.6.3 of the Regulations Governing ASTM Technical Committees, which requires that standards shall be updated by the end of the eighth year since the last approval date.

    1. Scope

    1.1 This test method covers a procedure to (a) identify asbestos in dust and (b) provide an estimate of the surface loading of asbestos in the sampled dust, reported as either the mass of asbestos per unit area of sampled surface or as the mass of asbestos per mass of sampled dust.

    1.1.1 If an estimate of asbestos structure counts is to be determined, the user is referred to Test Method D 5755.

    1.2 This test method describes the equipment and procedures necessary for sampling, by a microvacuum technique, non-airborne dust for levels of asbestos. The non-airborne sample is collected inside a standard filter membrane cassette from the sampling of a surface area for dust which may contain asbestos.

    1.2.1 This procedure uses a microvacuuming sampling technique. The collection efficiency of this technique is unknown. Variability of collection efficiency for any particular substrate and across different types of substrates is also unknown. The effects of sampling efficiency differences and variability on the interpretation of dust sampling measurements have not been determined.

    1.3 Asbestos identified by transmission electron microscopy (TEM) is based on morphology, selected area electron diffraction (SAED), and energy dispersive X-ray analysis (EDXA). Some information about structure size is also determined.

    1.4 This test method is generally applicable for an estimate of the surface loading of asbestos starting from approximately 0.24 pg of asbestos per square centimetre (assuming a minimum fiber dimension of 0.5 μm by 0.025 μm, see 17.8), but will vary with the analytical parameters noted in 17.8.

    1.4.1 The procedure outlined in this test method employs an indirect sample preparation technique. It is intended to disaggregate and disperse asbestos into fibrils and fiber bundles that can be more accurately identified, counted, and sized by transmission electron microscopy. However, as with all indirect sample preparation techniques, the asbestos observed for quantitation may not represent the physical form of the asbestos as sampled. More specifically, the procedure described neither creates not destroys asbestos, but it may alter the physical form of the mineral fibers.

    1.5 The values stated in SI units are to be regarded as the standard.

    1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.



    2. Referenced Documents (purchase separately) The documents listed below are referenced within the subject standard but are not provided as part of the standard.

    ASTM Standards

    D1193 Specification for Reagent Water

    D3195 Practice for Rotameter Calibration

    D5755 Test Method for Microvacuum Sampling and Indirect Analysis of Dust by Transmission Electron Microscopy for Asbestos Structure Number Surface Loading

    D6620 Practice for Asbestos Detection Limit Based on Counts

    E832 Specification for Laboratory Filter Papers

    ISO Standards

    ISO/CD13794 Ambient Air: Determination of Asbestos Fibres; Indirect-Transfer Transmission Electron Microscopy Procedure


    Referencing This Standard
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    DOI: 10.1520/D5756-02R08

    Citation Format

    ASTM D5756-02(2008), Standard Test Method for Microvacuum Sampling and Indirect Analysis of Dust by Transmission Electron Microscopy for Asbestos Mass Surface Loading (Withdrawn 2017), ASTM International, West Conshohocken, PA, 2008, www.astm.org

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