ASTM D5666 - 95(2019)

    Standard Test Method for Rubber Chemical Antidegradants—Purity of p-Phenylenediamine (PPD) Antidegradants by High Performance Liquid Chromatography

    Active Standard ASTM D5666 | Developed by Subcommittee: D11.11

    Book of Standards Volume: 09.01

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    Significance and Use

    5.1 This test method is designed to determine the purity of p-phenylenediamine antidegradants.

    5.2 Since the results of this test method are based on an integrated peak area as determined by HPLC, it is assumed that all analytes of interest are resolved from interfering peaks.

    1. Scope

    1.1 This test method covers the purity of Type I, II, and III p-phenylenediamine (PPD) antidegradants as described in Classification D4676 by high performance liquid chromatography (HPLC) using ultraviolet detection and external standard calculations.

    1.2 Expertise in HPLC is necessary to the successful application of this test method.

    1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

    1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.

    1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

    2. Referenced Documents (purchase separately) The documents listed below are referenced within the subject standard but are not provided as part of the standard.

    ASTM Standards

    D3853 Terminology Relating to Rubber and Rubber LaticesAbbreviations for Chemicals Used in Compounding

    D4483 Practice for Evaluating Precision for Test Method Standards in the Rubber and Carbon Black Manufacturing Industries

    D4676 Classification for Rubber Compounding MaterialsAntidegradants

    ISO Standards

    ISO5725 Precision of Test Methods

    ICS Code

    ICS Number Code 71.100.45 (Refrigerants and antifreezes)

    UNSPSC Code

    UNSPSC Code 12352100(Organic derivatives and substituted compounds)

    Referencing This Standard
    Link Here
    Link to Active (This link will always route to the current Active version of the standard.)

    DOI: 10.1520/D5666-95R19

    Citation Format

    ASTM D5666-95(2019), Standard Test Method for Rubber Chemical Antidegradants—Purity of p-Phenylenediamine (PPD) Antidegradants by High Performance Liquid Chromatography, ASTM International, West Conshohocken, PA, 2019,

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