If you are an ASTM Compass Subscriber and this document is part of your subscription, you can access it for free at ASTM Compass
    ASTM D4797 - 17

    Standard Test Methods for Gravimetric Analysis of White and Yellow Thermoplastic Pavement Marking

    Active Standard ASTM D4797 | Developed by Subcommittee: D01.44

    Book of Standards Volume: 06.02

      Format Pages Price  
    PDF 4 $46.00   ADD TO CART
    Hardcopy (shipping and handling) 4 $46.00   ADD TO CART
    Standard + Redline PDF Bundle 8 $54.00   ADD TO CART

    Significance and Use

    5.1 The function of these test methods is to define the percent of binder and retroreflective optics or non-retroreflective particles in the composition of the thermoplastic pavement marking as defined by the applicable specification for the manufacture of a specific thermoplastic pavement marking. The subsequent sample, as a result of ashing can be used to later test for the presence of titanium dioxide, lead chromate and possibly organic pigments.

    1. Scope

    1.1 These test methods cover procedures for the gravimetric analysis of the binder and hydrochloric Acid (HCL) insoluble particles in white and yellow thermoplastic pavement markings. The HCL insoluble particles can be retroreflective optics, such as glass beads or some other type of retroreflective optic, or non-retroreflective particles such as silica sand, or a combination of any two or more of these materials.

    1.2 This standard does not address the physical separation and the individual quantification of each component when a mixture of two or more HCL insoluble materials is present. Rather it requires the user to visually evaluate the HCL insoluble material (obtained from following this test method) and report the types of materials present.

    1.3 This standard does not purport to address the titanium dioxide or lead chromate pigment measurement (after ashing) which is detailed in Test Methods D1394 and D126.

    1.4 This standard will attempt to address the interference of organic pigments with the binder results.

    1.5 The analytical procedures appear in the following order:



    Percent Binder


    Percent Retroreflective Optics or
     Non-Retroreflective Particles


    1.6 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.

    1.7 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.

    1.8 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

    2. Referenced Documents (purchase separately) The documents listed below are referenced within the subject standard but are not provided as part of the standard.

    ASTM Standards

    D126 Test Methods for Analysis of Yellow, Orange, and Green Pigments Containing Lead Chromate and Chromium Oxide Green

    D1394 Test Methods for Chemical Analysis of White Titanium Pigments

    D7307 Practice for Sampling of Thermoplastic Traffic Marking Materials

    D7308 Practice for Sample Preparation of Thermoplastic Pavement Marking Materials

    E177 Practice for Use of the Terms Precision and Bias in ASTM Test Methods

    E691 Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method

    ICS Code

    ICS Number Code 93.080.30 (Road equipment and installations)

    UNSPSC Code

    UNSPSC Code

    Referencing This Standard
    Link Here
    Link to Active (This link will always route to the current Active version of the standard.)

    DOI: 10.1520/D4797-17

    Citation Format

    ASTM D4797-17, Standard Test Methods for Gravimetric Analysis of White and Yellow Thermoplastic Pavement Marking, ASTM International, West Conshohocken, PA, 2017, www.astm.org

    Back to Top