ASTM D4326 - 13
Standard Test Method for Major and Minor Elements in Coal and Coke Ash By X-Ray Fluorescence
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Significance and Use
5.1 A compositional analysis of ash is used in describing the quality of coal for its complete characterization. Ash composition is useful in predicting slagging and fouling characteristics of combusted materials as well as the potential utilization of ash by-products.
5.2 The chemical composition of laboratory prepared coal or coke ash is rarely, if ever, representative of the composition of the mineral matter in the coal because the ashing process can alter some minerals. However, it can approximate the composition of the fly ash and slag resulting from commercial combustion of coal or coke.
1. Scope
1.1 This test method covers the analysis of the commonly determined major and minor elements in ash from coal or coke using X-ray fluorescence (XRF) techniques.
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
2. Referenced Documents (purchase separately) The documents listed below are referenced within the subject standard but are not provided as part of the standard.
ASTM Standards
D121 Terminology of Coal and Coke
D346 Practice for Collection and Preparation of Coke Samples for Laboratory Analysis
D2013 Practice for Preparing Coal Samples for Analysis
D3173 Test Method for Moisture in the Analysis Sample of Coal and Coke
D3174 Test Method for Ash in the Analysis Sample of Coal and Coke from Coal
D5016 Test Method for Total Sulfur in Coal and Coke Combustion Residues Using a High-Temperature Tube Furnace Combustion Method with Infrared Absorption
D7348 Test Methods for Loss on Ignition (LOI) of Solid Combustion Residues
D7582 Test Methods for Proximate Analysis of Coal and Coke by Macro Thermogravimetric Analysis
E2 Methods of Preparation of Micrographs of Metals and Alloys (Including Recommended Practice for Photography As Applied to Metallography); Replaced by E 883
E11 Specification for Woven Wire Test Sieve Cloth and Test Sieves
ICS Code
ICS Number Code 75.160.10 (Solid fuels)
UNSPSC Code
UNSPSC Code 15101601(Coal); 15101604(Coke)
Referencing This Standard
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DOI: 10.1520/D4326
Citation Format
ASTM D4326-13, Standard Test Method for Major and Minor Elements in Coal and Coke Ash By X-Ray Fluorescence, ASTM International, West Conshohocken, PA, 2013, www.astm.org
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