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Significance and Use
5.1 The analysis of many types of water for metals using flame atomic absorption spectrophotometry, inductively coupled plasma emission spectrophotometry, direct current plasma emission spectrophotometry, or graphite furnace atomic absorption spectrophotometry necessitates the use of a digestion practice in order to ensure the proper statistical recovery of the metals from the sample matrix. The use of closed vessel microwave techniques will speed the complete recovery of metals from the water matrices and eliminate sample contamination from external sources.
1.1 This practice covers the general considerations for quantitative sample digestion for total metals in water using closed vessel microwave heating technique. This practice is applicable to surface, saline, domestic, and industrial wastewater.
1.2 Because of the differences among various makes and models of satisfactory instruments, no detailed operating instructions can be provided. Instead, the analyst should follow the instructions provided by the manufacturer of the particular instrument.
1.3 This practice can be used with the following ASTM standards, providing the user determines precision and bias based on this digestion practice: Test Method , Test Methods , Test Methods , Test Methods , Test Methods , Test Methods , Test Methods , Test Method , Practices , Test Methods , Test Methods , Practice , Test Method , Practice , Practice , and Test Method .
1.4 The values stated in SI units are to be regarded as standard. The values given in parentheses are mathematical conversion to inch-pound units that are provided for information only and are not considered standard.
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For specific hazard statements, see Section .
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
2. Referenced Documents (purchase separately) The documents listed below are referenced within the subject standard but are not provided as part of the standard.
U.S. EPA MethodU.S. EPA Method: Methods for Chemical Analysis of Water and WasteMarch 1979, Total Metals Digestion Procedure 4.1.3, page Metals 6 U.S. EPA Method: SW 846 Method 3015 Microwave Assisted Acid Digestion of Aqueous Samples and Extracts
D857 Test Method for Aluminum in Water
D858 Test Methods for Manganese in Water
D1068 Test Methods for Iron in Water
D1129 Terminology Relating to Water
D1193 Specification for Reagent Water
D1687 Test Methods for Chromium in Water
D1688 Test Methods for Copper in Water
D1691 Test Methods for Zinc in Water
D1886 Test Methods for Nickel in Water
D1976 Test Method for Elements in Water by Inductively-Coupled Argon Plasma Atomic Emission Spectroscopy
D3370 Practices for Sampling Water from Closed Conduits
D3557 Test Methods for Cadmium in Water
D3559 Test Methods for Lead in Water
D3856 Guide for Management Systems in Laboratories Engaged in Analysis of Water
D3919 Practice for Measuring Trace Elements in Water by Graphite Furnace Atomic Absorption Spectrophotometry
D4190 Test Method for Elements in Water by Direct-Current Plasma Atomic Emission Spectroscopy
D4453 Practice for Handling of High Purity Water Samples
D4691 Practice for Measuring Elements in Water by Flame Atomic Absorption Spectrophotometry
D5673 Test Method for Elements in Water by Inductively Coupled PlasmaMass Spectrometry
U.S. Code of Federal RegulationsCFR 1.030.10 Code of Federal Regulations, Volume 21
ICS Number Code 13.060.50 (Examination of water for chemical substances)
|Link to Active (This link will always route to the current Active version of the standard.)|
ASTM D4309-18, Standard Practice for Sample Digestion Using Closed Vessel Microwave Heating Technique for the Determination of Total Metals in Water, ASTM International, West Conshohocken, PA, 2018, www.astm.orgBack to Top