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Significance and Use
4.1 Sulfur is part of the ultimate analysis of coal and coke.
4.2 Results of the sulfur analysis are used for evaluation of coal preparation and cleaning, evaluation of potential sulfur emissions from coal and coke combustion or conversion processes, and evaluation of coal and coke quality in relation to contract specifications, as well as for scientific purposes.
4.3 The competency of laboratories with respect to use of this standard can be established through reference to Practice .
1.1 This test method covers the determination of sulfur in samples of coal or coke by high-temperature tube furnace combustion.
1.1.1 Two analysis methods are described.
1.2 When automated equipment is used, either method can be classified as an instrumental method.
1.3 The values stated in SI units are to be regarded as standard. The values given in parentheses after SI units are provided for information only and are not considered standard.
1.4 All percentages are percent mass fractions unless otherwise noted.
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
2. Referenced Documents (purchase separately) The documents listed below are referenced within the subject standard but are not provided as part of the standard.
ISO StandardISO 11722 ISO 5725-6 Accuracy (trueness and precision) of measurement methods and resultsPart 6: Use in practice of accuracy values
D346/D346M Practice for Collection and Preparation of Coke Samples for Laboratory Analysis
D2013/D2013M Practice for Preparing Coal Samples for Analysis
D3176 Practice for Ultimate Analysis of Coal and Coke
D3180 Practice for Calculating Coal and Coke Analyses from As-Determined to Different Bases
D7448 Practice for Establishing the Competence of Laboratories Using ASTM Procedures in the Sampling and Analysis of Coal and Coke
D7582 Test Methods for Proximate Analysis of Coal and Coke by Macro Thermogravimetric Analysis
E691 Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
ICS Number Code 75.160.10 (Solid fuels)
UNSPSC Code 15101601(Coal); 15101604(Coke)
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ASTM D4239-18e1, Standard Test Method for Sulfur in the Analysis Sample of Coal and Coke Using High-Temperature Tube Furnace Combustion, ASTM International, West Conshohocken, PA, 2018, www.astm.orgBack to Top