ASTM D244 - 09

    Standard Test Methods and Practices for Emulsified Asphalts

    Active Standard ASTM D244 | Developed by Subcommittee: D04.42

    Book of Standards Volume: 04.03

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    Significance and Use

    This test method measures the amount of water present in the emulsified asphalt, as distinguished from either bitumen or petroleum solvent.

    1. Scope

    1.1 These test methods and practices, given under the headings titled Composition, Consistency, Stability, and Examination of Residue, cover the examination of asphalt emulsions composed principally of a semisolid or liquid asphaltic base, water, and an emulsifying agent. The test methods cover the following tests and practices:

    Water Content4-10
    Residue and Oil Distillate by DistillationSee Test Method
    D 6997
    Residue by EvaporationSee Test Method
    D 6934
    Particle Charge of Cationic Emulsified AsphaltsSee Test Method
    D 7402
    Viscosity (Saybolt Furol)See Test Method
    D 7496
    DemulsibilitySee Test Method
    D 6936
    SettlementSee Test Method
    D 6930
    Cement MixingSee Test Method
    D 6935
    Sieve TestSee Test Method
    D 6933
    Aggregate CoatingSee Practice
    D 6998
    Miscibility with WaterSee Test Method
    D 6999
    FreezingSee Practice
    D 6929
    Coating Ability and Water Resistance11-18
    Storage Stability of Asphalt EmulsionSee Test Method
    D 6930
    Examination of Residue19-26
    Identification Test for Rapid Setting Cationic Emulsified Asphalt 27-34
    Identification of Cationic Slow Set EmulsionsSee Test Method
    D 7402
    Field Coating Test on Emulsified Asphalts35-40
    Emulsified Asphalt/Job Aggregate Coating Test41-46
    Density of Emulsified AsphaltSee Test Method
    D 6937
    Residue by Low-Temperature Vacuum DistillationSee Test Method
    D 7403

    1.2 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.

    1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

    4.1 This test method covers the procedure for determining the water content of an emulsified asphalt by reflux distillation using a water trap.

    11.1 This test method is intended to aid in the identification of asphalt emulsions suitable for mixing with coarse graded calcareous aggregates. It can be applied to other aggregates. (See Note 2).

    19.1 Tests for specific gravity, ash content, solubility in trichloroethylene, penetration, ductility and float test are suggested for examination of the emulsified asphalt residue obtained by distillation or evaporation (see Test Method D 6934 and Test Method D 6997).

    27.1 This practice covers a procedure for identifying rapid-setting cationic emulsified asphalts. Their inability to coat a specific silica sand distinguishes them from medium and slow setting cationic grades.

    35.1 This is a quick field test method to ascertain the compatibility of an emulsified asphalt with the job aggregate.

    41.1 This practice may be used to identify the adequacy of slow setting grade of emulsified asphalt to mix with and coat a dense and fine-graded job aggregate. It is a laboratory practice of screening emulsified asphalt candidates for mixing with and coating job aggregates and is not to be construed as a mix design test method.

    2. Referenced Documents (purchase separately) The documents listed below are referenced within the subject standard but are not provided as part of the standard.

    ASTM Standards

    C778 Specification for Sand

    D5 Test Method for Penetration of Bituminous Materials

    D70 Test Method for Density of Semi-Solid Bituminous Materials (Pycnometer Method)

    D86 Test Method for Distillation of Petroleum Products at Atmospheric Pressure

    D113 Test Method for Ductility of Bituminous Materials

    D128 Test Methods for Analysis of Lubricating Grease

    D139 Test Method for Float Test for Bituminous Materials

    D140 Practice for Sampling Bituminous Materials

    D977 Specification for Emulsified Asphalt

    D2042 Test Method for Solubility of Asphalt Materials in Trichloroethylene

    D2397 Specification for Cationic Emulsified Asphalt

    D3289 Test Method for Density of Semi-Solid and Solid Bituminous Materials (Nickel Crucible Method)

    D6929 Practice for Freezing of Emulsified Asphalts

    D6930 Test Method for Settlement and Storage Stability of Emulsified Asphalts

    D6933 Test Method for Oversized Particles in Emulsified Asphalts (Sieve Test)

    D6934 Test Method for Residue by Evaporation of Emulsified Asphalt

    D6935 Test Method for Determining Cement Mixing of Emulsified Asphalt

    D6936 Test Method for Determining Demulsibility of Emulsified Asphalt

    D6937 Test Method for Determining Density of Emulsified Asphalt

    D6997 Test Method for Distillation of Emulsified Asphalt

    D6998 Practice for Evaluating Aggregate Coating using Emulsified Asphalts

    D6999 Practice for Miscibility of Emulsified Asphalts

    D7402 Practice for Identifying Cationic Emulsified Asphalts

    D7403 Test Method for Determination of Residue of Emulsified Asphalt by Low Temperature Vacuum Distillation

    D7496 Test Method for Viscosity of Emulsified Asphalt by Saybolt Furol Viscometer

    E1 Specification for ASTM Liquid-in-Glass Thermometers

    E11 Specification for Woven Wire Test Sieve Cloth and Test Sieves

    E145 Specification for Gravity-Convection and Forced-Ventilation Ovens

    ICS Code

    ICS Number Code 91.100.50 (Binders. Sealing materials); 93.080.20 (Road construction materials)

    UNSPSC Code

    UNSPSC Code 30121601(Asphalt)

    Referencing This Standard
    Link Here
    Link to Active (This link will always route to the current Active version of the standard.)

    DOI: 10.1520/D0244-09

    Citation Format

    ASTM D244-09, Standard Test Methods and Practices for Emulsified Asphalts, ASTM International, West Conshohocken, PA, 2009,

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