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Significance and Use
4.1 Elemental constituents in potable water, receiving water, and wastewater need to be identified for support of effective pollution control programs. Test Methods A, B, and C provide the techniques necessary to make such measurements.
4.2 Nickel is considered to be relatively nontoxic to man and a limit for nickel is not included in the EPA National Interim Primary Drinking Water Regulations.6 The toxicity of nickel to aquatic life indicates tolerances that vary widely and that are influenced by species, pH, synergistic effects, and other factors.
4.3 Nickel is a silver-white metallic element seldom occur-ring in nature in the elemental form. Nickel salts are soluble and can occur as a leachate from nickel-bearing ores. Nickel salts are used in metal-plating and may be discharged to surface or ground waters.
1. Scope
1.1 These test methods 2, 3, 4 cover the atomic absorption determination of nickel in water and wastewaters. Three test methods are given as follows:
| Concentration | |
Test Method A—Atomic Absorption, Direct | | |
Test Method B—Atomic Absorption, Chelation-Extraction | | |
Test Method C—Atomic Absorption, Graphite Furnace | | |
1.2 Test Methods A, B, and C have been used successfully with reagent grade water and natural waters. Evaluation of Test Method C was also made in condensate from a medium Btu coal gasification process. It is the user's responsibility to ensure the validity of these test methods for other matrices.
1.3 The values stated in SI units are to be regarded as standard. The values given in parentheses are mathematical conversion to inch-pound units that are provided for information only and are not considered standard.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. For specific hazards statements, see Note 5, 11.8.1, 21.11, 23.7, and 23.10.
1.5 Two former colorimetric test methods were discontinued. Refer to Appendix X1 for historical information.
2. Referenced Documents (purchase separately) The documents listed below are referenced within the subject standard but are not provided as part of the standard.
ASTM Standards
D858 Test Methods for Manganese in Water
D1066 Practice for Sampling Steam
D1068 Test Methods for Iron in Water
D1129 Terminology Relating to Water
D1193 Specification for Reagent Water
D1687 Test Methods for Chromium in Water
D1688 Test Methods for Copper in Water
D1691 Test Methods for Zinc in Water
D2777 Practice for Determination of Precision and Bias of Applicable Test Methods of Committee D19 on Water
D3370 Practices for Sampling Water from Closed Conduits
D3557 Test Methods for Cadmium in Water
D3558 Test Methods for Cobalt in Water
D3559 Test Methods for Lead in Water
D3919 Practice for Measuring Trace Elements in Water by Graphite Furnace Atomic Absorption Spectrophotometry
D4841 Practice for Estimation of Holding Time for Water Samples Containing Organic and Inorganic Constituents
D5673 Test Method for Elements in Water by Inductively Coupled Plasma--Mass Spectrometry
D5810 Guide for Spiking into Aqueous Samples
D5847 Practice for Writing Quality Control Specifications for Standard Test Methods for Water Analysis
ICS Code
ICS Number Code 13.060.50 (Examination of water for chemical substances)
UNSPSC Code
UNSPSC Code 60104201(Water testing chemicals)
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DOI: 10.1520/D1886-14
Citation Format
ASTM D1886-14, Standard Test Methods for Nickel in Water, ASTM International, West Conshohocken, PA, 2014, www.astm.org
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