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    ASTM C1493-09

    Standard Test Method for Non-Destructive Assay of Nuclear Material in Waste by Passive and Active Neutron Counting Using a Differential Die-Away System (Withdrawn 2018)

    Withdrawn Standard: ASTM C1493-09 | Developed by Subcommittee: C26.10


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    Withdrawn Rationale:

    This test method covered a system that performs nondestructive assay (NDA) of uranium or plutonium, or both, using the active, differential die-away technique (DDT), and passive neutron coincidence counting.

    Formerly under the jurisdiction of Committee C26 on Nuclear Fuel Cycle, this test method was withdrawn in January 2018 in accordance with section 10.5.3.1 of the Regulations Governing ASTM Technical Committees, which requires that standards shall be updated by the end of the eighth year since the last approval date.

    1. Scope

    1.1 This test method covers a system that performs nondestructive assay (NDA) of uranium or plutonium, or both, using the active, differential die-away technique (DDT), and passive neutron coincidence counting. Results from the active and passive measurements are combined to determine the total amount of fissile and spontaneously-fissioning material in drums of scrap or waste. Corrections are made to the measurements for the effects of neutron moderation and absorption, assuming that the effects are averaged over the volume of the drum and that no significant lumps of nuclear material are present. These systems are most widely used to assay low-level and transuranic waste, but may also be used for the measurement of scrap materials. The examples given within this test method are specific to the second-generation Los Alamos National Laboratory (LANL) passive-active neutron assay system.

    1.1.1 In the active mode, the system measures fissile isotopes such as 235U and 239Pu. The neutrons from a pulsed, 14-MeV neutron generator are thermalized to induce fission in the assay item. Between generator pulses, the system detects prompt-fission neutrons emitted from the fissile material. The number of detected neutrons between pulses is proportional to the mass of fissile material. This method is called the differential die-away technique.

    1.1.2 In the passive mode, the system detects time-coincident neutrons emitted from spontaneously fissioning isotopes. The primary isotopes measured are 238Pu, 240Pu, and 242Pu; however, the system may be adapted for use on other spontaneously-fissioning isotopes as well, such as kilogram quantities of 238U. The number of coincident neutrons detected is proportional to the mass of spontaneously-fissioning material.

    1.2 The active mode is used to assay fissile material in the following ranges.

    1.2.1 For uranium-only bearing items, the DDT can measure the 235U content in the range from about 0.02 to over 100 g. Small mass uranium-bearing items are typically measured using the active mode and only large mass items are measured in passive mode.

    1.2.2 For plutonium-only bearing items, the DDT method measures the 239Pu content in the range between about 0.01 and 20 g.

    1.3 The passive mode is capable of assaying spontaneously-fissioning nuclei, over a nominal range from 0.05 to 15 g 240Pu equivalent.

    1.4 This test method requires knowledge of the relative abundances of the plutonium or uranium isotopes to determine the total plutonium or uranium mass.

    1.5 This test method will give biased results when the waste form does not meet the calibration specifications and the measurement assumptions presented in this test method regarding the requirements for a homogeneous matrix, uniform source distribution, and the absence of nuclear material lumps, to the extent that they effect the measurement.

    1.6 The complete active and passive assay of a 208 L drum is nominally 10 min or less but either mode can be extended to meet data quality objectives.

    1.7 Some improvements to this test method have been reported (1, 2, 3, 4). Discussions of these improvements are not included in this test method although improvements continue to occur.

    1.8 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

    1.9 This standard may involve hazardous materials, operations, and equipment. This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Specific precautionary statements are given in Section 8.



    2. Referenced Documents (purchase separately) The documents listed below are referenced within the subject standard but are not provided as part of the standard.

    ASTM Standards

    C1030 Test Method for Determination of Plutonium Isotopic Composition by Gamma-Ray Spectrometry

    C1207 Test Method for Nondestructive Assay of Plutonium in Scrap and Waste by Passive Neutron Coincidence Counting

    C1215 Guide for Preparing and Interpreting Precision and Bias Statements in Test Method Standards Used in the Nuclear Industry

    C1490 Guide for the Selection, Training and Qualification of Nondestructive Assay (NDA) Personnel

    C1592 Guide for Nondestructive Assay Measurements

    C1673 Terminology of C26.10 Nondestructive Assay Methods

    U.S. Government Documents

    USNRC Regulatory Guide 5.53 Qualification, Calibration, and Error Estimation Methods for Nondestructive Assay


    Referencing This Standard
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    DOI: 10.1520/C1493-09

    Citation Format

    ASTM C1493-09, Standard Test Method for Non-Destructive Assay of Nuclear Material in Waste by Passive and Active Neutron Counting Using a Differential Die-Away System (Withdrawn 2018), ASTM International, West Conshohocken, PA, 2009, www.astm.org

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