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This test method covers the determination of the concentration of technetium-99 in urine using inductively coupled plasma-mass spectrometry (ICP-MS). This test method can be used to support uranium enrichment and reclamation facility bioassay programs.
Formerly under the jurisdiction of Committee C26 on Nuclear Fuel Cycle, this test method was withdrawn in June 2011. This standard is being withdrawn without replacement due to its limited use by industry.
1.1 This test method covers the determination of the concentration of technetium-99 in urine using inductively coupled plasma-mass spectrometry (ICP-MS). This test method can be used to support uranium enrichment and reclamation facility bioassay programs.
1.2 The minimum detectable concentration for this test method, using a quadrupole ICP-MS, is approximately 1.0 ng/L (0.62 Bq/L).
This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
2. Referenced Documents (purchase separately) The documents listed below are referenced within the subject standard but are not provided as part of the standard.
C1009 Guide for Establishing a Quality Assurance Program for Analytical Chemistry Laboratories Within the Nuclear Industry
C1068 Guide for Qualification of Measurement Methods by a Laboratory Within the Nuclear Industry
C1128 Guide for Preparation of Working Reference Materials for Use in Analysis of Nuclear Fuel Cycle Materials
C1156 Guide for Establishing Calibration for a Measurement Method Used to Analyze Nuclear Fuel Cycle Materials
C1210 Guide for Establishing a Measurement System Quality Control Program for Analytical Chemistry Laboratories Within the Nuclear Industry
C1297 Guide for Qualification of Laboratory Analysts for the Analysis of Nuclear Fuel Cycle Materials
D1193 Specification for Reagent Water
Other StandardsHPS N13.30 Performance Criteria for Radiobioassay
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ASTM C1476-06, Standard Test Method for Analysis of Urine for Technetium-99 by Inductively Coupled Plasma-Mass Spectrometry (Withdrawn 2011), ASTM International, West Conshohocken, PA, 2006, www.astm.orgBack to Top