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This test method was used to measure the static splitting tensile strength of cylindrical specimens of brittle nuclear waste forms. It provided splitting tensile-strength data that could be used to compare the strength of waste forms when tests are done on one size of specimen.
Formerly under the jurisdiction of Committee C26 on Nuclear Fuel Cycle, this test method was withdrawn in September 2018. This standard is being withdrawn without replacement because the test method is not currently required to qualify waste forms for disposal per the Waste Acceptance Product Specification for Vitrified High-level Waste Forms (EM-WAPS), the Waste Acceptance System Requirements Document (DOE/RW-351P), or Land Disposal Restrictions.
1.1 This test method is used to measure the static splitting tensile strength of cylindrical specimens of brittle nuclear waste forms. It provides splitting tensile-strength data that can be used to compare the strength of waste forms when tests are done on one size of specimen.
1.2 The test method is applicable to glass, ceramic, and concrete waste forms that are sufficiently homogeneous (Note 1) but not to coated-particle, metal-matrix, bituminous, or plastic waste forms, or concretes with large-scale heterogeneities. Cementitious waste forms with heterogeneities >1 to 2 mm and 5 mm can be tested using this procedure provided the specimen size is increased from the reference size of 12.7 mm diameter by 6 mm length, to 51 mm diameter by 100 mm length, as recommended in Test Method C 496 and Practice C 192.
Note 1—Generally, the specimen structural or microstructural heterogeneities must be less than about one-tenth the diameter of the specimen.
1.3 This test method can be used as a quality control check on brittle waste forms and may be useful for optimizing waste form processing. Meaningful comparison of waste forms, however, requires data obtained on specimens of one size.
1.4 The values stated in SI units are to be regarded as the standard.
1.5 This standard may involve hazardous materials, operations, and equipment. This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. For specific hazard statements, see Section 7.
2. Referenced Documents (purchase separately) The documents listed below are referenced within the subject standard but are not provided as part of the standard.
C39/C39M Test Method for Compressive Strength of Cylindrical Concrete Specimens
C192/C192M Practice for Making and Curing Concrete Test Specimens in the Laboratory
C496/C496M Test Method for Splitting Tensile Strength of Cylindrical Concrete Specimens
C773 Test Method for Compressive (Crushing) Strength of Fired Whiteware Materials
D2938 Test Method for Unconfined Compressive Strength of Intact Rock Core Specimens
E4 Practices for Force Verification of Testing Machines
Society of Manufacturing EngineersGeometrical Tolerance Interpretations, SME Tool an
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ASTM C1144-89(2011), Standard Test Method for Splitting Tensile Strength for Brittle Nuclear Waste Forms (Withdrawn 2018), ASTM International, West Conshohocken, PA, 2011, www.astm.orgBack to Top