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    Materials Characterization by Dynamic and Modulated Thermal Analytical Techniques

    Riga AT, Judovits L
    Published: 2001

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    STP 1402 examines the latest dynamic and modulated thermal analytical techniques, including new interpretations and applications of Differential Scanning Calorimetry (DSC). The basis of many DSC methods is the modulation of temperature along with varying other parameters. Dynamic methods, including Dynamic Mechanical Analysis (DMA) and Dielectric Thermal Analysis (DETA), are also critiqued with new innovative applications. The mode of modulation, a sinusoidal wave or a saw tooth curve, affords the thermal analyst an opportunity to study a physical or chemical change in greater detail.

    15 peer reviewed papers cover:

    • Temperature Modulated Differential Scanning Calorimetry (TMDSC)

    • Use of TMDSC in Curing and Chemical Reactions

    • Measurement of the Glass Transition and Melting by Modulated and Comparative Techniques

    • General Modulated Techniques

    • Other Modulated Techniques

    • Dynamic Techniques DMA and DETA.

    Table of Contents

    Temperature-Modulated Calorimetry of Polymers with Single and multiple Frequencies to Determine Heat Capacities as Well as Reversible and Irreversible Transition Parameters

    Measurement of Crystallinity in Polymers Using Modulated Temperature Differential Scanning Calorimetry

    Crystallization of Polymers and the Rigid Amorphous Fraction Studied by the Temperature-Modulated Techniques TMDSC and TMDMA

    Evaluation of the Curing Process in a Fiber-Reinforced Epoxy Composite by Temperature-Modulated and Step Scan DSC and DMA

    Effects of TMDSC Variables on the Observed Glass Transitions of Elastomers- a Statistical Analysis

    Glass Transformation Studies of Vitreous As2Se3 by Temperature-Modulated DSC

    Comparison Between Modulated Differential Scanning Calorimetry (MDSC) and Dynamic Differential Scanning Calorimetry (DDSC)

    Modulated-Temperature Thermomechanical Measurements

    Obtaining Kinetic Parameters Using Modulated Temperature

    Analysis of Curing Using Simultaneous Dynamic Mechanical and Dielectric Measurements

    Characterization of Electrorheological Processes By Dielectric Thermal Analysis

    Characterization of Organic Surfactants and Dispersants by Frequency-Dependent Dielectric Thermal Analysis and Electrochemistry

    Development of Bismaleimide/Cyanate Ester Copolymers

    Application of Theory to Prediction and Analysis of Dynamic Mechanical Properties of Polymer Composites

    Glass Transition Temperature of Selected Polymers by TMDSC, DMTA and DETA Analyses

    Author Index

    Subject Index

    Committee: E37

    DOI: 10.1520/STP1402-EB

    ISBN-EB: 978-0-8031-5452-0

    ISBN-13: 978-0-8031-2887-3