SYMPOSIA PAPER Published: 01 January 1979
STP35008S

Glass Capillary Gas Chromatographic-Mass Spectrometric Analysis of Organics in Drinking Water Concentrates and Advanced Waste Treatment Water Concentrates-II

Source

A scheme has been established to analyze complex organic mixtures of water concentrates. It includes addition of deuterated internal standards to the concentrate, fractionation of the concentrate through a combination of extraction under both acidic and basic conditions, partitioning on a short silica gel column, and finally, analysis of the partitioned fractions as well as the unpartitioned concentrate by glass capillary gas chromatography using a flame ionization detector (GC-FID) and glass capillary gas chromatography coupled to a mass spectrometer (GC-MS). The GC-FID and GC-MS analyses are conducted on two types of wall-coated open-tubular glass capillary GC columns, one containing a nonpolar liquid phase (SP2100) and the other a polar liquid phase (SP1000).

Author Information

Lin, DCK
Battelle Columbus Laboratories, Columbus, Ohio
Foltz, RL
Battelle Columbus Laboratories, Columbus, Ohio
Lucas, SV
Battelle Columbus Laboratories, Columbus, Ohio
Petersen, BA
Battelle Columbus Laboratories, Columbus, Ohio
Slivon, LE
Battelle Columbus Laboratories, Columbus, Ohio
Melton, RG
U.S. Environmental Protection Agency, Health Effect Research Laboratory, Cincinnati, Ohio
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Details
Developed by Committee: D19
Pages: 68–84
DOI: 10.1520/STP35008S
ISBN-EB: 978-0-8031-4753-9
ISBN-13: 978-0-8031-0508-9