You are being redirected because this document is part of your ASTM Compass® subscription.
    This document is part of your ASTM Compass® subscription.


    The Defect Structure of Ion and Neutron Irradiated YBa2Cu3O7-δ Single Crystals

    Published: Jan 1992

      Format Pages Price  
    PDF (236K) 7 $25   ADD TO CART
    Complete Source PDF (28M) 1299 $264   ADD TO CART


    Using transmission electron microscopy techniques, we have begun a program to study cascade defects in the high-Tc superconductor YBa2Cu3O7-δ. In situ ion irradiations in the high-voltage electron microscope (HVEM) accelerator facility at Argonne National Laboratory were performed to simulate low-dose neutron irradiation at both room temperature and at 40 K. Diffraction contrast experiments performed in two-beam dark field conditions using different operating reflections indicated defect cascades with hydrostatic pressure-like strain fields. Visible cascade defect yields ranged from 0.3 to 1.0, depending on incident ion mass. High-resolution micrographs revealed that at least some of these cascades have recrystallized regions that have rotated with respect to the surrounding lattice. Samples which were neutron irradiated to doses sufficient to produce overlapped cascades show a “cellular” structure of good crystalline material surrounded by highly defective or amorphous cell walls. It is suggested that the recrystallization observed in isolated cascade defects produced by low-dose ion irradiation provides the mechanism for the formation of the cellular structure at high damage levels. We will suggest correlations between neutron irradiation responses of the microstructure and the critical current density measured magnetically and also electrical resistivity measurements of the superconducting to insulating transition.


    neutron irradiation, ion irradiation, cascade defects, YBa, 2, Cu, 3, O, 7-δ, single crystals

    Author Information:

    Frischherz, MC
    Graduate student, Science and Technology Center for SuperconductivityArgonne National Laboratory, Argonne, IL

    Kirk, MA
    Metallurgist, Argonne National Laboratory, Argonne, IL

    Liu, JZ
    Visiting scientist, Argonne National LaboratoryUniversity of California, Davis, CA

    Zhang, JP
    Post doctorate, Science and Technology Center for SuperconductivityNorthwestern University, Technical Institute, Evanston, IL

    Weber, HW
    Professor, Atominstitut der osterreichischen Universitaten, Wien,

    Committee/Subcommittee: E10.08

    DOI: 10.1520/STP17906S