(Received 16 May 1988; accepted 25 July 1988)
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Heroin and three structurally related isomers were studied. The configurational assignments of the structural isomers supported from nuclear magnetic resonance and mass spectrometry data are discussed. Infrared spectroscopy spectra are also presented. Gas chromatography procedures using packed and capillary systems demonstrated how the isomers could be best fully resolved.
Forensic chemist, Drug Enforcement Administration, South Central Laboratory, Dallas, TX
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