Journal Published Online: 01 September 1988
Volume 33, Issue 5

Identification of Sugars in Explosive Residues by Gas Chromatography-Mass Spectrometry

CODEN: JFSCAS

Abstract

Chlorate/sugar mixtures are commonly used in improvised explosive devices. Sugars in the burnt chlorate/sugar residues are derivatized using trimethylsilylimidazole (TMSI) in pyridine. The resulting sugar-TMS derivatives are analyzed by gas chromatography-mass spectrometry. The presence of chlorates or byproducts of the chlorate/sugar reaction do not interfere in this process.

Author Information

Nowicki, J
Illinois State Police, Bureau of Forensic Sciences, Maywood, IL
Pauling, S
Home Office Forensic Science Laboratory, Huntingdon, Cambridgeshire, England
Pages: 8
Price: $25.00
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Stock #: JFS12561J
ISSN: 0022-1198
DOI: 10.1520/JFS12561J