Journal Published Online: 01 January 1984
Volume 29, Issue 1

An Analytical Study of Illicit Lysergide

CODEN: JFSCAS

Abstract

A procedure for the analysis of lysergide, applicable to the illicit material dispersed on paper sheets and in tablets is described. Thin-layer and high performance liquid chromatography are used to separate lysergide from related compounds. Attention is drawn to the limitations of infrared spectroscopy for distinguishing between the salt and base forms of lysergide. Ion chromatography is used to separate the anions present in illicit samples. The quantities of any anions present that form stable salts with lysergide are compared with the amount of lysergide in the sample, from which the salt form of the presentation is deduced.

Author Information

McDonald, P
Laboratory of the Government Chemist Cornwall House, London, United Kingdom
Martin, CF
Laboratory of the Government Chemist Cornwall House, London, United Kingdom
Woods, DJ
Laboratory of the Government Chemist Cornwall House, London, United Kingdom
Baker, PB
Laboratory of the Government Chemist Cornwall House, London, United Kingdom
Gough, TA
Laboratory of the Government Chemist Cornwall House, London, United Kingdom
Pages: 11
Price: $25.00
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Details
Stock #: JFS11642J
ISSN: 0022-1198
DOI: 10.1520/JFS11642J