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1.1 This test method covers the quantitative determination of the distribution of particle sizes of the fine-grained portion of soils. The sedimentation or hydrometer method is used to determine the particle-size distribution (gradation) of the material that is finer than the No. 200 (75-µm) sieve and larger than about 0.2-µm. The test is performed on material passing the No. 10 (2.0-mm) or finer sieve and the results are presented as the mass percent finer versus the log of the particle diameter.
1.2 This method can be used to evaluate the fine-grained fraction of a soil with a wide range of particle sizes by combining the sedimentation results with a sieve analysis resulting in the complete gradation curve. The method can also be used when there are no coarse-grained particles or when the gradation of the coarse-grained material is not required or not needed.
Note 1: The significant digits recorded in this test method preclude obtaining the grain size distribution of materials that do not contain a significant amount of fines. For example, clean sands will not yield detectable amounts of silt and clay sized particles, and therefore should not be tested with this method. The minimum amount of fines in the sedimentation specimen is 15 g.
1.3 When combining the results of the sedimentation and sieve tests, the procedure for obtaining the material for the sedimentation analysis and calculations for combining the results will be provided by the more general test method, such as Test Methods ( ).
Note 2: Subcommittee D18.03 is currently developing a new test method “Test Method for Particle-Size Analysis of Soils Combining the Sieve and Sedimentation Techniques.”
1.4 The terms “soil” and “material” are used interchangeably throughout the standard.
1.5 The sedimentation analysis is based on the concept that larger particles will fall through a fluid faster than smaller particles. Stokes’ Law gives a governing equation used to determine the terminal velocity of a spherical particle falling through a stationary liquid. The terminal velocity is proportional to the square of the particle diameter. Therefore, particles are sorted by size in both time and position when settling in a container of liquid.
1.5.1 Stokes’ Law has several assumptions which are: the particles are spherical and smooth; there is no interference between the particles; there is no difference between the current in the middle of the container and the sides; flow is laminar; and the particles have the same density. These assumptions are applied to soil particles of various shapes and sizes.
1.6 A hydrometer is used to measure the fluid density and determine the quantity of particles in suspension at a specific time and position. The density of the soil-water suspension depends upon the concentration and specific gravity of the soil particles and the amount of dispersant added. Each hydrometer measurement at an elapsed time is used to calculate the percentage of particles finer than the diameter given by Stokes’ Law. The series of readings provide the distribution of material mass as a function of particle size.
1.7 This test method does not cover procurement of the sample or processing of the sample prior to obtaining the reduced sample in any detail. It is assumed that the sample is obtained using appropriate methods and is representative of site materials or conditions. It is also assumed that the sample has been processed such that the reduced sample accurately reflects the particle-size distribution (gradation) of this finer fraction of the material.
1.8 Material Processing—Material is tested in the moist or as-received state unless the material is received in an air-dried state. The moist preparation method shall be used to obtain a sedimentation test specimen from the reduced sample. Air-dried preparation is only allowed when the material is received in the air-dried state. The method to be used may be specified by the requesting authority; however, the moist preparation method shall be used for referee testing.
1.9 This test method is not applicable for the following soils:
1.9.1 Soils containing fibrous peat.
1.9.2 Soils containing less than approximately 5 % of fine-grained material ( ).
1.9.3 Soils containing extraneous matter, such as organic solvents, oil, asphalt, wood fragments, or similar items ( ).
Note 3: If extraneous matter, such as wood, can be easily removed by hand, it is permissible to do so. However, there may be cases where the extraneous matter is being evaluated as part of the material and it should not be removed from the material.
1.9.4 Materials that contain cementitious components, such as cement, fly ash, lime, or other stabilization admixtures.
1.10 This test method may not produce consistent test results within and between laboratories for the following soils. To test these soils, this test method must be adapted and these adaptations documented.
1.10.1 Soils that flocculate during sedimentation. Such materials may need to be treated to reduce salinity or alter the pH of the suspension.
1.10.2 Friable soils in which processing changes the gradation of the soil. Typical examples of these soils are some residual soils, most weathered shales, and some weakly cemented soils.
1.10.3 Soils that will not readily disperse, such as glauconitic clays or some dried plastic clays.
1.11 Samples that are not soils, but are made up of particles may be tested using this method. The applicable sections above should be used in applying this standard.
1.12 Units—The values stated in SI units are to be regarded as standard. Except the sieve designations, they are identified using the “alternative” system in accordance with Practice , such as 3-in. and No. 200, instead of the “standard” of 75-mm and 75-µm, respectively. Reporting of test results in units other than SI shall not be regarded as non-conformance with this test method. The use of balances or scales recording pounds of mass (lbm) shall not be regarded as nonconformance with this standard.
1.13 All observed and calculated values shall conform to the guidelines for significant digits and rounding established in Practice , unless superseded by this test method.
1.13.1 The procedures used to specify how data are collected/recorded and calculated in the standard are regarded as the industry standard. In addition, they are representative of the significant digits that generally should be retained. The procedures used do not consider material variation, purpose for obtaining the data, special purpose studies, or any considerations for the user’s objectives; and it is common practice to increase or reduce significant digits of reported data to be commensurate with these considerations. It is beyond the scope of these test methods to consider significant digits used in analysis methods for engineering data.
1.14 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
2. Referenced Documents (purchase separately) The documents listed below are referenced within the subject standard but are not provided as part of the standard.
D653 Terminology Relating to Soil, Rock, and Contained Fluids
D854 Test Methods for Specific Gravity of Soil Solids by Water Pycnometer
D1140 Test Methods for Determining the Amount of Material Finer than 75-m (No. 200) Sieve in Soils by Washing
D2216 Test Methods for Laboratory Determination of Water (Moisture) Content of Soil and Rock by Mass
D2487 Practice for Classification of Soils for Engineering Purposes (Unified Soil Classification System)
D2488 Practice for Description and Identification of Soils (Visual-Manual Procedure)
D3740 Practice for Minimum Requirements for Agencies Engaged in Testing and/or Inspection of Soil and Rock as Used in Engineering Design and Construction
D4220/D4220M Practices for Preserving and Transporting Soil Samples
D4318 Test Methods for Liquid Limit, Plastic Limit, and Plasticity Index of Soils
D4753 Guide for Evaluating, Selecting, and Specifying Balances and Standard Masses for Use in Soil, Rock, and Construction Materials Testing
D6026 Practice for Using Significant Digits in Geotechnical Data
D6913 Test Methods for Particle-Size Distribution (Gradation) of Soils Using Sieve Analysis
E11 Specification for Woven Wire Test Sieve Cloth and Test Sieves
E100 Specification for ASTM Hydrometers
E126 Test Method for Inspection, Calibration, and Verification of ASTM Hydrometers
ICS Number Code 13.080.20 (Physical properties of soil)
UNSPSC Code 11111501(Soil); 41113024(Hydrometers)
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ASTM D7928-16e1, Standard Test Method for Particle-Size Distribution (Gradation) of Fine-Grained Soils Using the Sedimentation (Hydrometer) Analysis, ASTM International, West Conshohocken, PA, 2016, www.astm.orgBack to Top