ASTM D7214-07a

    Standard Test Method for Determination of the Oxidation of Used Lubricants by FT-IR Using Peak Area Increase Calculation

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    1. Scope

    1.1 This test method covers the determination of the oxidation of used lubricants by FT-IR (Fourier Transform Infrared Spectroscopy). It measures the concentration change of constituents containing a carbonyl function that have formed during the oxidation of the lubricant.

    1.2 This test method may be used to indicate relative changes that occur in an oil under oxidizing conditions. The test method is not intended to measure an absolute oxidation property that can be used to predict performance of an oil in service.

    1.3 This test method was developed for transmission oils which have been degraded either in service, or in a laboratory test, for example a bulk oxidation test. It may be used for other in-service oils, but the stated precision may not apply.

    1.4 The results of this test method may be affected by the presence of other components with an absorbance band in the zone of 16001800 cm-1. Low PAI values may be difficult to determine in those cases. Section 6 describes these possible interferences in more detail.

    1.5 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

    1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

    2. Referenced Documents (purchase separately) The documents listed below are referenced within the subject standard but are not provided as part of the standard.

    ASTM Standards

    D4057 Practice for Manual Sampling of Petroleum and Petroleum Products

    D4177 Practice for Automatic Sampling of Petroleum and Petroleum Products

    D6299 Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance

    D7418 Practice for Set-Up and Operation of Fourier Transform Infrared (FT-IR) Spectrometers for In-Service Oil Condition Monitoring

    E131 Terminology Relating to Molecular Spectroscopy

    CEC Standard

    CEC L-48-A-00 Oxidation Stability of Lubricating Oils Used in Automotive Transmissions by Artificial Aging Available from Coordinating European Council (CEC), c/o Interlynk Administrative Services, Ltd., P.O. Box 6475, Earl Shilton, Leicester, LE9 9ZB, U.K.

    ICS Code

    ICS Number Code 75.100 (Lubricants, industrial oils and related products)

    UNSPSC Code

    UNSPSC Code 15121500(Lubricating preparations)

    Referencing This Standard
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    DOI: 10.1520/D7214-07A

    Citation Format

    ASTM D7214-07a, Standard Test Method for Determination of the Oxidation of Used Lubricants by FT-IR Using Peak Area Increase Calculation, ASTM International, West Conshohocken, PA, 2007,

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