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1.1 These test methods cover the determination of ammonia nitrogen, exclusive of organic nitrogen, in water. Two test methods are included as follows:
|Test Method A—Direct Nesslerization||7 to 15|
|Test Method B—Ion Selective Electrode||16 to 24|
1.2 Test Method A is used for the routine determination of ammonia in steam condensates and demineralizer effluents.
1.3 Test Method B is applicable to the determination of ammonia nitrogen in the range from 0.5 to 1000 mg NH3N/L directly in reagent and effluent waters. Higher concentrations can be determined following dilution. The reported lower range is based on multiple-operator precision. Lower limits have been obtained by two of the twelve laboratories participating in the round robin.
1.4 Both test methods A and B are applicable to surface and industrial waters and wastewaters following distillation. The test method for distillation given in Appendix X1 has been used in the past to meet requirements for predistillation of samples being analyzed for ammonia.
1.5 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
1.7 The distillation method now appears as Appendix X1 and is provided as nonmandatory information only. The automated colorimetric phenate method has been discontinued.
7.1 This test method is suitable for the rapid routine determination of ammonia nitrogen in steam condensates and demineralized water. See Appendix X1 for the distillation test method.
16.1 This test method is applicable to the measurement of ammonia in reagent and effluent water.
2. Referenced Documents (purchase separately) The documents listed below are referenced within the subject standard but are not provided as part of the standard.
D1066 Practice for Sampling Steam
D1129 Terminology Relating to Water
D1193 Specification for Reagent Water
D2777 Practice for Determination of Precision and Bias of Applicable Test Methods of Committee D19 on Water
D3370 Practices for Sampling Water from Closed Conduits
D5810 Guide for Spiking into Aqueous Samples
D5847 Practice for Writing Quality Control Specifications for Standard Test Methods for Water Analysis
E60 Practice for Analysis of Metals, Ores, and Related Materials by Spectrophotometry
E275 Practice for Describing and Measuring Performance of Ultraviolet and Visible Spectrophotometers
APHA StandardStandard Methods for the Examination of Water and Waste Water
ICS Number Code 13.060.50 (Examination of water for chemical substances)
|Link to Active (This link will always route to the current Active version of the standard.)|
ASTM D1426-08, Standard Test Methods for Ammonia Nitrogen In Water, ASTM International, West Conshohocken, PA, 2008, www.astm.orgBack to Top