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1.1 These test methods cover the determination of fluoride ion in water. The following two test methods are given:Sections Test Method A (Distillation) 7 to 14 Test Method B (Ion Selective Electrode) 15 to 22
1.2 Test Method A covers the accurate measurement of total fluoride in water through isolation of the fluoride by distillation and subsequent measurement in the distillate by use of the ion selective electrode method. The procedure covers the range from 0.1 to 2.6 mg/L of fluoride.
1.3 Test Method B covers the accurate measurement of simple fluoride ion in water by means of an ion selective electrode. With this test method, distillation is eliminated because the electrode is not affected by the interferences common to colorimetric procedures. Concentrations of fluoride from 0.1 to 1000 mg/L may be measured.
1.4 This standard does not purport to address all of the safety problems, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. For a specific precautionary statement, see 12.1.2.
1.5 Former Test Method A, SPADNS Photometric Procedure, was discontinued. Refer to Appendix X1 for historical information.
2. Referenced Documents (purchase separately) The documents listed below are referenced within the subject standard but are not provided as part of the standard.
D1066 Practice for Sampling Steam
D1129 Terminology Relating to Water
D1193 Specification for Reagent Water
D2777 Practice for Determination of Precision and Bias of Applicable Test Methods of Committee D19 on Water
D3370 Practices for Sampling Water from Closed Conduits
D4127 Terminology Used with Ion-Selective Electrodes
D5810 Guide for Spiking into Aqueous Samples
D5847 Practice for Writing Quality Control Specifications for Standard Test Methods for Water Analysis
ICS Number Code 13.060.50 (Examination of water for chemical substances)
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ASTM D1179-99, Standard Test Methods for Fluoride Ion in Water, ASTM International, West Conshohocken, PA, 1999, www.astm.orgBack to Top