Table of Contents

D3712-18 Standard Test Method of Analysis of Oil-Soluble Sulfonates by Liquid Chromatography

D3764-19 Standard Practice for Validation of the Performance of Process Stream Analyzer Systems

D3827-92(2012) Standard Test Method for Estimation of Solubility of Gases in Petroleum and Other Organic Liquids

D3828-16a Standard Test Methods for Flash Point by Small Scale Closed Cup Tester

D3829-18 Standard Test Method for Predicting the Borderline Pumping Temperature of Engine Oil

D3831-12(2017) Standard Test Method for Manganese in Gasoline By Atomic Absorption Spectroscopy

D3944-12(2017) Standard Test Method for Solidification Point of Petroleum Wax

D3948-14(2018) Standard Test Method for Determining Water Separation Characteristics of Aviation Turbine Fuels by Portable Separometer

D4006-16e1 Standard Test Method for Water in Crude Oil by Distillation

D4007-11(2016)e1 Standard Test Method for Water and Sediment in Crude Oil by the Centrifuge Method (Laboratory Procedure)

D4042-93(2014) Standard Test Method for Sampling and Testing for Ash and Total Iron in Steel Mill Dispersions of Rolling Oils

D4045-15 Standard Test Method for Sulfur in Petroleum Products by Hydrogenolysis and Rateometric Colorimetry

D4046-14(2019) Standard Test Method for Alkyl Nitrate in Diesel Fuels by Spectrophotometry

D4047-18 Standard Test Method for Phosphorus in Lubricating Oils and Additives by Quinoline Phosphomolybdate Method

D4048-19a Standard Test Method for Detection of Copper Corrosion from Lubricating Grease

D4049-16 Standard Test Method for Determining the Resistance of Lubricating Grease to Water Spray

D4051-10(2015) Standard Practice for Preparation of Low-Pressure Gas Blends

D4052-18a Standard Test Method for Density, Relative Density, and API Gravity of Liquids by Digital Density Meter

D4054-19 Standard Practice for Evaluation of New Aviation Turbine Fuels and Fuel Additives

D4055-04(2019) Standard Test Method for Pentane Insolubles by Membrane Filtration

D4056-16 Standard Test Method for Estimation of Solubility of Water in Hydrocarbon and Aliphatic Ester Lubricants

D4057-19 Standard Practice for Manual Sampling of Petroleum and Petroleum Products

D4072-98(2018) Standard Test Method for Toluene-Insoluble (TI) Content of Tar and Pitch

D4170-16 Standard Test Method for Fretting Wear Protection by Lubricating Greases

D4171-16a Standard Specification for Fuel System Icing Inhibitors

D4172-18 Standard Test Method for Wear Preventive Characteristics of Lubricating Fluid (Four-Ball Method)

D4174-17 Standard Practice for Cleaning, Flushing, and Purification of Petroleum Fluid Hydraulic Systems

D4175-19 Standard Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants

D4176-04(2014) Standard Test Method for Free Water and Particulate Contamination in Distillate Fuels (Visual Inspection Procedures)

D4177-16e1 Standard Practice for Automatic Sampling of Petroleum and Petroleum Products

D4178-82(2017) Standard Practice for Calibrating Moisture Analyzers

D4289-13(2014)e1 Standard Test Method for Elastomer Compatibility of Lubricating Greases and Fluids

D4290-15 Standard Test Method for Determining the Leakage Tendencies of Automotive Wheel Bearing Grease Under Accelerated Conditions

D4291-04(2017) Standard Test Method for Trace Ethylene Glycol in Used Engine Oil

D4292-17 Standard Test Method for Determination of Vibrated Bulk Density of Calcined Petroleum Coke

D4293-15e1 Standard Specification for Phosphate Ester Based Fluids for Turbine Lubrication and Steam Turbine Electro-Hydraulic Control (EHC) Applications

D4294-16e1 Standard Test Method for Sulfur in Petroleum and Petroleum Products by Energy Dispersive X-ray Fluorescence Spectrometry

D4296-18 Standard Practice for Sampling Pitch

D4304-17 Standard Specification for Mineral and Synthetic Lubricating Oil Used in Steam or Gas Turbines

D4306-15 Standard Practice for Aviation Fuel Sample Containers for Tests Affected by Trace Contamination

D4307-17 Standard Practice for Preparation of Liquid Blends for Use as Analytical Standards

D4308-13 Standard Test Method for Electrical Conductivity of Liquid Hydrocarbons by Precision Meter

D4310-10(2015) Standard Test Method for Determination of Sludging and Corrosion Tendencies of Inhibited Mineral Oils

D4312-15 Standard Test Method for Toluene-Insoluble (TI) Content of Tar and Pitch (Short Method)

D4377-00(2011) Standard Test Method for Water in Crude Oils by Potentiometric Karl Fischer Titration

D4378-13 Standard Practice for In-Service Monitoring of Mineral Turbine Oils for Steam, Gas, and Combined Cycle Turbines

D4418-17 Standard Practice for Receipt, Storage, and Handling of Fuels for Gas Turbines

D4419-90(2015) Standard Test Method for Measurement of Transition Temperatures of Petroleum Waxes by Differential Scanning Calorimetry (DSC)

D4422-19 Standard Test Method for Ash in Analysis of Petroleum Coke

D4423-10(2015) Standard Test Method for Determination of Carbonyls in C4 Hydrocarbons

D4424-09(2014) Standard Test Method for Butylene Analysis by Gas Chromatography

D4425-19 Standard Test Method for Oil Separation from Lubricating Grease by Centrifuging (Koppers Method)

D4485-18a Standard Specification for Performance of Active API Service Category Engine Oils

D4486-18 Standard Test Method for Kinematic Viscosity of Volatile and Reactive Liquids

D4529-17 Standard Test Method for Estimation of Net Heat of Combustion of Aviation Fuels

D4530-15 Standard Test Method for Determination of Carbon Residue (Micro Method)

D4539-17 Standard Test Method for Filterability of Diesel Fuels by Low-Temperature Flow Test (LTFT)

D4616-95(2018) Standard Test Method for Microscopical Analysis by Reflected Light and Determination of Mesophase in a Pitch

D4625-16e1 Standard Test Method for Middle Distillate Fuel Storage Stability at 43 °C (110 °F)

D4626-95(2015) Standard Practice for Calculation of Gas Chromatographic Response Factors

D4627-12(2017) Standard Test Method for Iron Chip Corrosion for Water–Miscible Metalworking Fluids

D4628-16 Standard Test Method for Analysis of Barium, Calcium, Magnesium, and Zinc in Unused Lubricating Oils by Atomic Absorption Spectrometry

D4629-17 Standard Test Method for Trace Nitrogen in Liquid Hydrocarbons by Syringe/Inlet Oxidative Combustion and Chemiluminescence Detection

D4636-17 Standard Test Method for Corrosiveness and Oxidation Stability of Hydraulic Oils, Aircraft Turbine Engine Lubricants, and Other Highly Refined Oils

D4682-18 Standard Specification for Miscibility with Gasoline and Fluidity of Two-Stroke-Cycle Gasoline Engine Lubricants

D4683-17 Standard Test Method for Measuring Viscosity of New and Used Engine Oils at High Shear Rate and High Temperature by Tapered Bearing Simulator Viscometer at 150 °C

D4684-18 Standard Test Method for Determination of Yield Stress and Apparent Viscosity of Engine Oils at Low Temperature

D4693-07(2017) Standard Test Method for Low-Temperature Torque of Grease-Lubricated Wheel Bearings

D4715-98(2017) Standard Test Method for Coking Value of Tar and Pitch (Alcan)

D4737-10(2016) Standard Test Method for Calculated Cetane Index by Four Variable Equation

D4739-17 Standard Test Method for Base Number Determination by Potentiometric Hydrochloric Acid Titration

D4740-19 Standard Test Method for Cleanliness and Compatibility of Residual Fuels by Spot Test

D4741-18 Standard Test Method for Measuring Viscosity at High Temperature and High Shear Rate by Tapered-Plug Viscometer

D4742-17 Standard Test Method for Oxidation Stability of Gasoline Automotive Engine Oils by Thin-Film Oxygen Uptake (TFOUT)

D4746-14e1 Standard Test Method for Determination of Quinoline Insolubles (QI) in Tar and Pitch by Pressure Filtration

D4806-19a Standard Specification for Denatured Fuel Ethanol for Blending with Gasolines for Use as Automotive Spark-Ignition Engine Fuel

D4807-05(2015) Standard Test Method for Sediment in Crude Oil by Membrane Filtration

D4808-17 Standard Test Methods for Hydrogen Content of Light Distillates, Middle Distillates, Gas Oils, and Residua by Low-Resolution Nuclear Magnetic Resonance Spectroscopy

D4809-18 Standard Test Method for Heat of Combustion of Liquid Hydrocarbon Fuels by Bomb Calorimeter (Precision Method)

D4814-19 Standard Specification for Automotive Spark-Ignition Engine Fuel

D4815-15b Standard Test Method for Determination of MTBE, ETBE, TAME, DIPE, tertiary-Amyl Alcohol and C1 to C4 Alcohols in Gasoline by Gas Chromatography

D4857-12 Standard Test Method for Determination of the Ability of Lubricants to Minimize Ring Sticking and Piston Deposits in Two-Stroke-Cycle Gasoline Engines Other Than Outboards

D4858-13 Standard Test Method for Determination of the Tendency of Lubricants to Promote Preignition in Two-Stroke-Cycle Gasoline Engines

D4859-13 Standard Specification for Lubricants for Two-Stroke-Cycle Spark-Ignition Gasoline Engines-TC

D4860-14(2019) Standard Test Method for Free Water and Particulate Contamination in Middle Distillate Fuels (Clear and Bright Numerical Rating)

D4863-13 Standard Test Method for Determination of Lubricity of Two-Stroke-Cycle Gasoline Engine Lubricants

D4865-19 Standard Guide for Generation and Dissipation of Static Electricity in Petroleum Fuel Systems

D4868-17 Standard Test Method for Estimation of Net and Gross Heat of Combustion of Hydrocarbon Burner and Diesel Fuels

D4870-18 Standard Test Method for Determination of Total Sediment in Residual Fuels

D4871-11(2016) Standard Guide for Universal Oxidation/Thermal Stability Test Apparatus

D4892-14(2019)e1 Standard Test Method for Density of Solid Pitch (Helium Pycnometer Method)

D4893-94(2015)e1 Standard Test Method for Determination of Pitch Volatility

D4898-16 Standard Test Method for Insoluble Contamination of Hydraulic Fluids by Gravimetric Analysis

D4927-15 Standard Test Methods for Elemental Analysis of Lubricant and Additive Components—Barium, Calcium, Phosphorus, Sulfur, and Zinc by Wavelength-Dispersive X-Ray Fluorescence Spectroscopy

D4928-12(2018) Standard Test Method for Water in Crude Oils by Coulometric Karl Fischer Titration

D4929-19 Standard Test Method for Determination of Organic Chloride Content in Crude Oil

D4930-06(2017) Standard Test Method for Dust Control Material on Calcined Petroleum Coke

D4931-06(2017) Standard Test Method for Gross Moisture in Green Petroleum Coke

D4950-14 Standard Classification and Specification for Automotive Service Greases

D4951-14 Standard Test Method for Determination of Additive Elements in Lubricating Oils by Inductively Coupled Plasma Atomic Emission Spectrometry

D4952-12(2017) Standard Test Method for Qualitative Analysis for Active Sulfur Species in Fuels and Solvents (Doctor Test)

D4953-15 Standard Test Method for Vapor Pressure of Gasoline and Gasoline-Oxygenate Blends (Dry Method)

D4998-13 Standard Test Method for Evaluating Wear Characteristics of Tractor Hydraulic Fluids

D5001-10(2014) Standard Test Method for Measurement of Lubricity of Aviation Turbine Fuels by the Ball-on-Cylinder Lubricity Evaluator (BOCLE)

D5002-18e1 Standard Test Method for Density, Relative Density, and API Gravity of Crude Oils by Digital Density Analyzer

D5003-19 Standard Test Method for Hardgrove Grindability Index (HGI) of Petroleum Coke

D5004-11(2017) Standard Test Method for Real Density of Calcined Petroleum Coke by Xylene Displacement

D5006-11(2016) Standard Test Method for Measurement of Fuel System Icing Inhibitors (Ether Type) in Aviation Fuels

D5018-18 Standard Test Method for Shear Viscosity of Coal-Tar and Petroleum Pitches

D5056-17 Standard Test Method for Trace Metals in Petroleum Coke by Atomic Absorption

D5059-14(2019) Standard Test Methods for Lead in Gasoline by X-Ray Spectroscopy

D5133-15 Standard Test Method for Low Temperature, Low Shear Rate, Viscosity/Temperature Dependence of Lubricating Oils Using a Temperature-Scanning Technique

D5134-13(2017) Standard Test Method for Detailed Analysis of Petroleum Naphthas through n-Nonane by Capillary Gas Chromatography

D5182-97(2014) Standard Test Method for Evaluating the Scuffing Load Capacity of Oils (FZG Visual Method)

D5183-05(2016) Standard Test Method for Determination of the Coefficient of Friction of Lubricants Using the Four-Ball Wear Test Machine

D5184-12(2017) Standard Test Methods for Determination of Aluminum and Silicon in Fuel Oils by Ashing, Fusion, Inductively Coupled Plasma Atomic Emission Spectrometry, and Atomic Absorption Spectrometry

D5185-18 Standard Test Method for Multielement Determination of Used and Unused Lubricating Oils and Base Oils by Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES)

D5186-19 Standard Test Method for Determination of the Aromatic Content and Polynuclear Aromatic Content of Diesel Fuels By Supercritical Fluid Chromatography

D5187-10(2015)e1 Standard Test Method for Determination of Crystallite Size (Lc) of Calcined Petroleum Coke by X-Ray Diffraction

D5188-16 Standard Test Method for Vapor-Liquid Ratio Temperature Determination of Fuels (Evacuated Chamber and Piston Based Method)

D5191-19 Standard Test Method for Vapor Pressure of Petroleum Products and Liquid Fuels (Mini Method)

D5234-92(2017) Standard Guide for Analysis of Ethylene Product

D5236-18a Standard Test Method for Distillation of Heavy Hydrocarbon Mixtures (Vacuum Potstill Method)

D5273-18 Standard Guide for Analysis of Propylene Concentrates

D5274-00(2014) Standard Guide for Analysis of 1,3–Butadiene Product

D5275-17 Standard Test Method for Fuel Injector Shear Stability Test (FISST) for Polymer Containing Fluids

D5291-16 Standard Test Methods for Instrumental Determination of Carbon, Hydrogen, and Nitrogen in Petroleum Products and Lubricants

D5293-17a Standard Test Method for Apparent Viscosity of Engine Oils and Base Stocks Between –10 °C and –35 °C Using Cold-Cranking Simulator

D5303-19 Standard Test Method for Trace Carbonyl Sulfide in Propylene by Gas Chromatography

D5304-15 Standard Test Method for Assessing Middle Distillate Fuel Storage Stability by Oxygen Overpressure

D5305-18 Standard Test Method for Determination of Ethyl Mercaptan in LP-Gas Vapor

D5306-92(2018) Standard Test Method for Linear Flame Propagation Rate of Lubricating Oils and Hydraulic Fluids

D5372-17 Standard Guide for Evaluation of Hydrocarbon Heat Transfer Fluids

D5384-14(2019) Standard Test Methods for Chlorine in Used Petroleum Products (Field Test Kit Method)

D5441-98(2017) Standard Test Method for Analysis of Methyl Tert-Butyl Ether (MTBE) by Gas Chromatography

D5442-17 Standard Test Method for Analysis of Petroleum Waxes by Gas Chromatography

D5443-14(2018) Standard Test Method for Paraffin, Naphthene, and Aromatic Hydrocarbon Type Analysis in Petroleum Distillates Through 200 °C by Multi-Dimensional Gas Chromatography

D5452-12 Standard Test Method for Particulate Contamination in Aviation Fuels by Laboratory Filtration

D5453-19a Standard Test Method for Determination of Total Sulfur in Light Hydrocarbons, Spark Ignition Engine Fuel, Diesel Engine Fuel, and Engine Oil by Ultraviolet Fluorescence

D5481-13 Standard Test Method for Measuring Apparent Viscosity at High-Temperature and High-Shear Rate by Multicell Capillary Viscometer

D5482-07(2013) Standard Test Method for Vapor Pressure of Petroleum Products (Mini Method—Atmospheric)

D5483-05(2015) Standard Test Method for Oxidation Induction Time of Lubricating Greases by Pressure Differential Scanning Calorimetry

D5500-18 Standard Test Method for Vehicle Evaluation of Unleaded Automotive Spark-Ignition Engine Fuel for Intake Valve Deposit Formation

D5501-12(2016) Standard Test Method for Determination of Ethanol and Methanol Content in Fuels Containing Greater than 20% Ethanol by Gas Chromatography

D5502-00(2015) Standard Test Method for Apparent Density by Physical Measurements of Manufactured Anode and Cathode Carbon Used by the Aluminum Industry

D5534-94(2018) Standard Test Method for Vapor-Phase Rust-Preventing Characteristics of Hydraulic Fluids

D5579-19 Standard Test Method for Evaluating the Thermal Stability of Manual Transmission Lubricants in a Cyclic Durability Test

D5580-15 Standard Test Method for Determination of Benzene, Toluene, Ethylbenzene, p/m-Xylene, o-Xylene, C9 and Heavier Aromatics, and Total Aromatics in Finished Gasoline by Gas Chromatography

D5598-18 Standard Test Method for Evaluating Unleaded Automotive Spark-Ignition Engine Fuel for Electronic Port Fuel Injector Fouling

D5599-18 Standard Test Method for Determination of Oxygenates in Gasoline by Gas Chromatography and Oxygen Selective Flame Ionization Detection

D5600-17 Standard Test Method for Trace Metals in Petroleum Coke by Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES)

D5621-19 Standard Test Method for Sonic Shear Stability of Hydraulic Fluids

D5622-17 Standard Test Methods for Determination of Total Oxygen in Gasoline and Methanol Fuels by Reductive Pyrolysis

D5623-19 Standard Test Method for Sulfur Compounds in Light Petroleum Liquids by Gas Chromatography and Sulfur Selective Detection

D5662-19 Standard Test Method for Determining Automotive Gear Oil Compatibility with Typical Oil Seal Elastomers

D5704-17 Standard Test Method for Evaluation of the Thermal and Oxidative Stability of Lubricating Oils Used for Manual Transmissions and Final Drive Axles

D5705-15 Standard Test Method for Measurement of Hydrogen Sulfide in the Vapor Phase Above Residual Fuel Oils

D5706-16 Standard Test Method for Determining Extreme Pressure Properties of Lubricating Greases Using a High-Frequency, Linear-Oscillation (SRV) Test Machine

D5707-16 Standard Test Method for Measuring Friction and Wear Properties of Lubricating Grease Using a High-Frequency, Linear-Oscillation (SRV) Test Machine

D5708-15 Standard Test Methods for Determination of Nickel, Vanadium, and Iron in Crude Oils and Residual Fuels by Inductively Coupled Plasma (ICP) Atomic Emission Spectrometry

D5709-09(2015) Standard Test Method for Sieve Analysis of Petroleum Coke

D5760-19 Standard Specification for Performance of Manual Transmission Gear Lubricants

D5761-96(2017) Standard Practice for Emulsification/Suspension of Multiphase Fluid Waste Materials

D5762-18a Standard Test Method for Nitrogen in Liquid Hydrocarbons, Petroleum and Petroleum Products by Boat-Inlet Chemiluminescence

D5763-11(2016) Standard Test Method for Oxidation and Thermal Stability Characteristics of Gear Oils Using Universal Glassware

D5769-15 Standard Test Method for Determination of Benzene, Toluene, and Total Aromatics in Finished Gasolines by Gas Chromatography/Mass Spectrometry

D5770-11(2017) Standard Test Method for Semiquantitative Micro Determination of Acid Number of Lubricating Oils During Oxidation Testing

D5771-17 Standard Test Method for Cloud Point of Petroleum Products and Liquid Fuels (Optical Detection Stepped Cooling Method)

D5772-17 Standard Test Method for Cloud Point of Petroleum Products and Liquid Fuels (Linear Cooling Rate Method)

D5773-17e1 Standard Test Method for Cloud Point of Petroleum Products and Liquid Fuels (Constant Cooling Rate Method)

D5797-18 Standard Specification for Methanol Fuel Blends (M51–M85) for Methanol-Capable Automotive Spark-Ignition Engines

D5798-19b Standard Specification for Ethanol Fuel Blends for Flexible-Fuel Automotive Spark-Ignition Engines

D5799-95(2014) Standard Test Method for Determination of Peroxides in Butadiene

D5800-19 Standard Test Method for Evaporation Loss of Lubricating Oils by the Noack Method

D5842-17 Standard Practice for Sampling and Handling of Fuels for Volatility Measurement

D5845-01(2016) Standard Test Method for Determination of MTBE, ETBE, TAME, DIPE, Methanol, Ethanol and tert-Butanol in Gasoline by Infrared Spectroscopy

D5846-07(2017) Standard Test Method for Universal Oxidation Test for Hydraulic and Turbine Oils Using the Universal Oxidation Test Apparatus

D5853-17a Standard Test Method for Pour Point of Crude Oils

D5854-19a Standard Practice for Mixing and Handling of Liquid Samples of Petroleum and Petroleum Products

D5863-00a(2016) Standard Test Methods for Determination of Nickel, Vanadium, Iron, and Sodium in Crude Oils and Residual Fuels by Flame Atomic Absorption Spectrometry

D5864-18 Standard Test Method for Determining Aerobic Aquatic Biodegradation of Lubricants or Their Components

D5949-16 Standard Test Method for Pour Point of Petroleum Products (Automatic Pressure Pulsing Method)

D5950-14 Standard Test Method for Pour Point of Petroleum Products (Automatic Tilt Method)

D5966-13 Standard Test Method for Evaluation of Engine Oils for Roller Follower Wear in Light-Duty Diesel Engine

D5967-17 Standard Test Method for Evaluation of Diesel Engine Oils in T-8 Diesel Engine

D5968-19 Standard Test Method for Evaluation of Corrosiveness of Diesel Engine Oil at 121 °C

D5969-11(2016) Standard Test Method for Corrosion-Preventive Properties of Lubricating Greases in Presence of Dilute Synthetic Sea Water Environments

D5972-16 Standard Test Method for Freezing Point of Aviation Fuels (Automatic Phase Transition Method)

D5983-18 Standard Specification for Methyl Tertiary-Butyl Ether (MTBE) for Blending With Gasolines for Use as Automotive Spark-Ignition Engine Fuel

D5984-11(2017) Standard Test Method for Semi-Quantitative Field Test Method for Base Number in New and Used Lubricants by Color-Indicator Titration

D5985-02(2014) Standard Test Method for Pour Point of Petroleum Products (Rotational Method)

D5986-96(2015) Standard Test Method for Determination of Oxygenates, Benzene, Toluene, C8–C 12 Aromatics and Total Aromatics in Finished Gasoline by Gas Chromatography/Fourier Transform Infrared Spectroscopy

D6006-17 Standard Guide for Assessing Biodegradability of Hydraulic Fluids

D6021-12(2017) Standard Test Method for Measurement of Total Hydrogen Sulfide in Residual Fuels by Multiple Headspace Extraction and Sulfur Specific Detection

D6022-06(2012) Standard Practice for Calculation of Permanent Shear Stability Index

D6045-12(2017) Standard Test Method for Color of Petroleum Products by the Automatic Tristimulus Method

D6046-18 Standard Classification of Hydraulic Fluids for Environmental Impact

D6074-15 Standard Guide for Characterizing Hydrocarbon Lubricant Base Oils

D6078-04(2016) Standard Test Method for Evaluating Lubricity of Diesel Fuels by the Scuffing Load Ball-on-Cylinder Lubricity Evaluator (SLBOCLE)

D6079-18 Standard Test Method for Evaluating Lubricity of Diesel Fuels by the High-Frequency Reciprocating Rig (HFRR)

D6080-18a Standard Practice for Defining the Viscosity Characteristics of Hydraulic Fluids

D6081-19 Standard Practice for Aquatic Toxicity Testing of Lubricants: Sample Preparation and Results Interpretation

D6082-12(2017) Standard Test Method for High Temperature Foaming Characteristics of Lubricating Oils

D6120-97(2017)e1 Standard Test Method for Electrical Resistivity of Anode and Cathode Carbon Material at Room Temperature

D6121-19 Standard Test Method for Evaluation of Load-Carrying Capacity of Lubricants Under Conditions of Low Speed and High Torque Used for Final Hypoid Drive Axles