ASTM F326 - 96(2012)

    Standard Test Method for Electronic Measurement for Hydrogen Embrittlement From Cadmium-Electroplating Processes

    Active Standard ASTM F326 | Developed by Subcommittee: F07.04

    Book of Standards Volume: 15.03


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    ASTM F326

    Significance and Use

    5.1 Hydrogen is evolved during metal electrodeposition in aqueous baths. Some of this hydrogen enters parts during plating. If the absorbed hydrogen is at a level presenting embrittlement hazards to high-strength steel, it is removed by baking parts after plating to expel this hydrogen. However, the lack of plate porosity itself may block hydrogen egress. Thus, it becomes important to know both the relative amount of hydrogen absorbed and the plate porosity.

    5.2 This test provides a quantitative control number for cadmium plate porosity that can be used to control a cadmium plating process and the status of cadmium-plated hardware. It can also be used for plating process troubleshooting and research and development to determine the effects on plate porosity by process variables, contaminants, and materials. When used to control a critical process, control numbers for plate porosity must be determined by correlation with stress rupture specimens or other acceptable standards.

    5.3 There is no prime standard for plate porosity. For this reason, two ovens must be used, with tests alternated between ovens. Data from the ovens are compared to ensure no equipment change has occurred.

    1. Scope

    1.1 This test method covers an electronic hydrogen detection instrument procedure for measurement of plating permeability to hydrogen. This method measures a variable related to hydrogen absorbed by steel during plating and to the hydrogen permeability of the plate during post plate baking. A specific application of this method is controlling cadmium-plating processes in which the plate porosity relative to hydrogen is critical, such as cadmium on high-strength steel.

    1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. For specific hazard statement, see Section 8.

    1.3 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.


    2. Referenced Documents (purchase separately) The documents listed below are referenced within the subject standard but are not provided as part of the standard.

    ASTM Standards

    D1193 Specification for Reagent Water

    F519 Test Method for Mechanical Hydrogen Embrittlement Evaluation of Plating/Coating Processes and Service Environments


    ICS Code

    ICS Number Code 25.220.40 (Metallic coatings)

    UNSPSC Code

    UNSPSC Code


    DOI: 10.1520/F0326-96R12

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