ASTM F2328M - 07(2014)

    Standard Test Method for Determining Decarburization and Carburization in Hardened and Tempered Threaded Steel Bolts, Screws and Studs (Metric)

    Active Standard ASTM F2328M | Developed by Subcommittee: F16.01

    Book of Standards Volume: 01.08


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    ASTM F2328M

    Significance and Use

    4.1 Decarburization and carburization are two surface conditions created, either intentionally or unintentionally, as with a pre-existing condition created during the rod rolling process, the rod/wire annealing process, or while heat treating threaded steel products. Too much of either will adversely affect the safety and performance of the threaded product. Therefore, limits have been established for four different product groups: the harder and greater the tensile strength of the product, the more susceptible to failure the product becomes if these limits are exceeded.

    4.2 When testing to a particular product specification that lists the dimensions and microindentation data to be used, that data shall take precedence over the tables in this test method.

    4.3 There are only two viable methods available to detect these deficiencies: either by the visual method or the microindentation method. Both methods are used for routine inspections when evaluations are conducted at a single location on the product sample. Because an evaluation at a specific location may not be representative of the whole part, the referee method employs the microindentation method taken as an average of evaluations conducted on four adjacent threads. This procedure significantly reduces random test variables when compared to testing on a single thread.˙

    4.4 Specifying this test method does not specify or imply that testing shall be for either decarburization or carburization alone or for both conditions. When either test method is performed, both conditions will be apparent and shall be reported. For example, if an order is placed to test for decarburization and none is found but the presence of decarburization is detected, it shall be reported on the test report that carburization was found.

    1. Scope

    1.1 This test method covers procedures for measuring, classifying, and determining the presence of decarburization and carburization in the threaded section of hardened and tempered metric steel bolts, screws, studs, and similar parts which have been heated to facilitate fabrication or to modify its mechanical properties. This test method is not intended to address products which are intentionally carburized to achieve specific results.

    1.2 Two routine methods are described for measuring the limits of and determining the presence of decarburization or carburization; the Optical Method and the Microindentation Method 1. Either method is appropriate for routine examinations. The Microindentation Method 2 shall be considered the referee method.

    1.3 For the purpose of these tests, there are four classes of hardened and tempered steel products for which specific measurements must be made with respect to their physical properties.

    1.4 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

    1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.


    2. Referenced Documents (purchase separately) The documents listed below are referenced within the subject standard but are not provided as part of the standard.

    ASTM Standards

    A574M Specification for Alloy Steel Socket-Head Cap Screws (Metric)

    E3 Guide for Preparation of Metallographic Specimens

    E384 Test Method for Knoop and Vickers Hardness of Materials

    F835M Specification for Alloy Steel Socket Button and Flat Countersunk Head Cap Screws (Metric)

    F912M Specification for Alloy Steel Socket Set Screws (Metric)

    F1789 Terminology for F16 Mechanical Fasteners


    ICS Code

    ICS Number Code 21.060.01 (Fasteners in general); 77.140.20 (Steels of high quality)

    UNSPSC Code

    UNSPSC Code 31160000(Hardware)


    DOI: 10.1520/F2328M

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